Z-Asp(OBzl)-OPyCl

Base Information

• Chemical Name: Z-Asp(OBzl)-OPyCl
• CAS No.: 122751-41-1
• Molecular Formula: C₂₄H₂₁ClN₂O₆
• Molecular Weight: 468.894

Synonyms:Z-Asp(OBzl)-OPyCl

Chemical Property of Z-Asp(OBzl)-OPyCl

Chemical Property:

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Technology Process of Z-Asp(OBzl)-OPyCl

There total 1 articles about Z-Asp(OBzl)-OPyCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.3%

6-chloro-2-hydroxypyridine (16879-02-0) + Z-Asp(OBzl)-OH (3479-47-8) → Z-Asp(OBzl)-OPyCl (122751-41-1)

Guidance literature:

With dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 4 ℃;

DOI:10.1248/cpb.37.46

Reference yield: 92.5%

methyl (2S)-2-amino-3-phenylpropanoate (2577-90-4) + Z-Asp(OBzl)-OPyCl (122751-41-1) → Z-Asp(OBzl)-Phe-OMe (5262-07-7)

Guidance literature:

In 1,4-dioxane; Ambient temperature;

DOI:10.1248/cpb.37.46

Reference yield: 79.1%

(S)-serine methyl ester (2788-84-3) + Z-Asp(OBzl)-OPyCl (122751-41-1) → Z-Asp(OBzl)-Ser-OMe (51871-02-4)

Guidance literature:

In 1,4-dioxane; Ambient temperature;

DOI:10.1248/cpb.37.46

upstream raw materials:

6-chloro-2-hydroxypyridine

Z-Asp(OBzl)-OH

Downstream raw materials:

Z-Asp(OBzl)-Ser-OMe

Z-Asp(OBzl)-Phe-OMe

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