ingenol 3-(5-methyl-3-(2-chloro-6-fluoro-phenyl)-isoxazole-4-carboxylate)

Base Information

Chemical Name:ingenol 3-(5-methyl-3-(2-chloro-6-fluoro-phenyl)-isoxazole-4-carboxylate)
CAS No.:1383547-12-3
Molecular Formula:C₃₁H₃₃ClFNO₇
Molecular Weight:586.057
Hs Code.:

Synonyms:ingenol 3-(5-methyl-3-(2-chloro-6-fluoro-phenyl)-isoxazole-4-carboxylate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ingenol 3-(5-methyl-3-(2-chloro-6-fluoro-phenyl)-isoxazole-4-carboxylate)

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Technology Process of ingenol 3-(5-methyl-3-(2-chloro-6-fluoro-phenyl)-isoxazole-4-carboxylate)

There total 3 articles about ingenol 3-(5-methyl-3-(2-chloro-6-fluoro-phenyl)-isoxazole-4-carboxylate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1383548-20-6
ingenol-5,20-acetonide-3-(5-methyl-3-(2-chloro-6-fluoro-phenyl)-isoxazole-4-carboxylate)

: 1383547-12-3
ingenol 3-(5-methyl-3-(2-chloro-6-fluoro-phenyl)-isoxazole-4-carboxylate)

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃; Inert atmosphere;

Reference yield:

: 30220-46-3
ingenol

: 1383547-12-3
ingenol 3-(5-methyl-3-(2-chloro-6-fluoro-phenyl)-isoxazole-4-carboxylate)

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / 0.42 h / 20 °C

2: dmap; N-ethyl-N,N-diisopropylamine / acetonitrile / 150 °C / Microwave irradiation

3: hydrogenchloride / water; tetrahydrofuran / 20 °C / Inert atmosphere

With hydrogenchloride; dmap; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; water; acetonitrile;

Reference yield:

: 77573-43-4
(6S,6aR,7aR,9R,9aS,12S,12aR,12bR)-12,12a-dihydroxy-2,2,7,7,9,11-hexamethyl-4,6,6a,7,7a,8,9,12,12a,12b-decahydro-6,9a-methanocyclopenta[9,10]cyclopropa[5,6]cyclodeca[1,2-d][1,3]dioxin-13-one

: 1383547-12-3
ingenol 3-(5-methyl-3-(2-chloro-6-fluoro-phenyl)-isoxazole-4-carboxylate)

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; N-ethyl-N,N-diisopropylamine / acetonitrile / 150 °C / Microwave irradiation

2: hydrogenchloride / water; tetrahydrofuran / 20 °C / Inert atmosphere

With hydrogenchloride; dmap; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; water; acetonitrile;