ingenol-5,20-acetonide-3-(5-methyl-3-(2-chloro-6-fluoro-phenyl)-isoxazole-4-carboxylate)

Base Information

Chemical Name:ingenol-5,20-acetonide-3-(5-methyl-3-(2-chloro-6-fluoro-phenyl)-isoxazole-4-carboxylate)
CAS No.:1383548-20-6
Molecular Formula:C₃₄H₃₇ClFNO₇
Molecular Weight:626.122
Hs Code.:

Synonyms:ingenol-5,20-acetonide-3-(5-methyl-3-(2-chloro-6-fluoro-phenyl)-isoxazole-4-carboxylate)

Suppliers and Price of ingenol-5,20-acetonide-3-(5-methyl-3-(2-chloro-6-fluoro-phenyl)-isoxazole-4-carboxylate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ingenol-5,20-acetonide-3-(5-methyl-3-(2-chloro-6-fluoro-phenyl)-isoxazole-4-carboxylate)

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Technology Process of ingenol-5,20-acetonide-3-(5-methyl-3-(2-chloro-6-fluoro-phenyl)-isoxazole-4-carboxylate)

There total 2 articles about ingenol-5,20-acetonide-3-(5-methyl-3-(2-chloro-6-fluoro-phenyl)-isoxazole-4-carboxylate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77573-43-4
(6S,6aR,7aR,9R,9aS,12S,12aR,12bR)-12,12a-dihydroxy-2,2,7,7,9,11-hexamethyl-4,6,6a,7,7a,8,9,12,12a,12b-decahydro-6,9a-methanocyclopenta[9,10]cyclopropa[5,6]cyclodeca[1,2-d][1,3]dioxin-13-one

: 69399-79-7
3-(2-chloro-6-fluorophenyl)-5-methylisoxazole-4-carbonyl chloride

: 1383548-20-6
ingenol-5,20-acetonide-3-(5-methyl-3-(2-chloro-6-fluoro-phenyl)-isoxazole-4-carboxylate)

Guidance literature:: With dmap; N-ethyl-N,N-diisopropylamine; In acetonitrile; at 150 ℃; Microwave irradiation;

Reference yield:

: 30220-46-3
ingenol

: 1383548-20-6
ingenol-5,20-acetonide-3-(5-methyl-3-(2-chloro-6-fluoro-phenyl)-isoxazole-4-carboxylate)

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / 0.42 h / 20 °C

2: dmap; N-ethyl-N,N-diisopropylamine / acetonitrile / 150 °C / Microwave irradiation

With dmap; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; In acetonitrile;