2-allyl-7-(5-{4-[tris-(4-tert-butyl-phenyl)-methyl]-phenoxy}-pentyl)-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

Base Information

• Chemical Name: 2-allyl-7-(5-{4-[tris-(4-tert-butyl-phenyl)-methyl]-phenoxy}-pentyl)-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone
• CAS No.: 760951-11-9
• Molecular Formula: C₅₉H₆₂N₂O₅
• Molecular Weight: 879.152

Synonyms:2-allyl-7-(5-{4-[tris-(4-tert-butyl-phenyl)-methyl]-phenoxy}-pentyl)-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

Chemical Property of 2-allyl-7-(5-{4-[tris-(4-tert-butyl-phenyl)-methyl]-phenoxy}-pentyl)-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

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Technology Process of 2-allyl-7-(5-{4-[tris-(4-tert-butyl-phenyl)-methyl]-phenoxy}-pentyl)-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

There total 3 articles about 2-allyl-7-(5-{4-[tris-(4-tert-butyl-phenyl)-methyl]-phenoxy}-pentyl)-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

4-[tris-(4-tert-butylphenyl)methyl]phenol (143998-20-3) + 2-allyl-7-(5-hydroxy-pentyl)-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone → 2-allyl-7-(5-{4-[tris-(4-tert-butyl-phenyl)-methyl]-phenoxy}-pentyl)-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone (760951-11-9)

Guidance literature:

With di-isopropyl azodicarboxylate; triphenylphosphine; In dichloromethane; at 20 ℃; for 16h;

DOI:10.1021/ja048080k

Reference yield:

5-hydroxypentylamine (2508-29-4) → 2-allyl-7-(5-{4-[tris-(4-tert-butyl-phenyl)-methyl]-phenoxy}-pentyl)-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone (760951-11-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 36 percent / dimethylformamide / 2 h / 120 °C

2: 71 percent / PPh₃; DIAD / CH₂Cl₂ / 16 h / 20 °C

With di-isopropyl azodicarboxylate; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide; 2: Mitsunobu reaction;

DOI:10.1021/ja048080k

Reference yield:

1,4,5,8-naphthalenetetracarboxylic dianhydride (81-30-1) → 2-allyl-7-(5-{4-[tris-(4-tert-butyl-phenyl)-methyl]-phenoxy}-pentyl)-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone (760951-11-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 36 percent / dimethylformamide / 2 h / 120 °C

2: 71 percent / PPh₃; DIAD / CH₂Cl₂ / 16 h / 20 °C

With di-isopropyl azodicarboxylate; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide; 2: Mitsunobu reaction;

DOI:10.1021/ja048080k

upstream raw materials:

4-[tris-(4-tert-butylphenyl)methyl]phenol

5-hydroxypentylamine

1,4,5,8-naphthalenetetracarboxylic dianhydride

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