(2',3',4',6'-tetra-O-benzyl-β-D-galactopyranosyl)methylamine

Base Information

• Chemical Name: (2',3',4',6'-tetra-O-benzyl-β-D-galactopyranosyl)methylamine
• CAS No.: 204069-49-8
• Molecular Formula: C₃₅H₃₉NO₅
• Molecular Weight: 553.698
• Mol file: 204069-49-8.mol

Synonyms:(2',3',4',6'-tetra-O-benzyl-β-D-galactopyranosyl)methylamine

Chemical Property of (2',3',4',6'-tetra-O-benzyl-β-D-galactopyranosyl)methylamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (2',3',4',6'-tetra-O-benzyl-β-D-galactopyranosyl)methylamine

There total 6 articles about (2',3',4',6'-tetra-O-benzyl-β-D-galactopyranosyl)methylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

1-Deoxy-2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl cyanide (113019-40-2) → 1-C-formyl-3,4,6-tri-O-benzyl-D-galactal + (2',3',4',6'-tetra-O-benzyl-β-D-galactopyranosyl)methylamine (204069-49-8)

Guidance literature:

1-Deoxy-2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl cyanide; With diisobutylaluminium hydride; In dichloromethane; at -78 ℃; for 0.5h;

With water; ammonium chloride; In dichloromethane;

DOI:10.1016/j.carres.2011.04.019

Reference yield: 45.0%

1-Deoxy-2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl cyanide (113019-40-2) → (2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)methanal (140397-46-2) + 1-C-formyl-3,4,6-tri-O-benzyl-D-galactal + (2',3',4',6'-tetra-O-benzyl-β-D-galactopyranosyl)methylamine (204069-49-8)

Guidance literature:

1-Deoxy-2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl cyanide; With diisobutylaluminium hydride; In dichloromethane; at -78 ℃; for 0.5h;

With water; ammonium chloride; In dichloromethane;

DOI:10.1016/j.carres.2011.04.019

Reference yield:

(2',3',4',6'-tetra-O-benzyl-β-D-galactopyranosyl)methyl azide (474081-58-8) → (2',3',4',6'-tetra-O-benzyl-β-D-galactopyranosyl)methylamine (204069-49-8)

Guidance literature:

With hydrogen; palladium dihydroxide; In ethyl acetate; at 20 ℃; for 0.333333h;

DOI:10.1021/jo0202076

upstream raw materials:

1-Deoxy-2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl cyanide

(2',3',4',6'-tetra-O-benzyl-β-D-galactopyranosyl)methyl azide

(2',3',4',6'-tetra-O-benzyl-β-D-galactopyranosyl)methyl alcohol

(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)methanal

Downstream raw materials:

(2',3',4',6'-tetra-O-benzyl-β-D-galactopyranosyl)methylurea

(4S)-1-[(2',3',4',6'-tetra-O-benzyl-β-D-galactopyranosyl)methyl]-6-methyl-2-oxo-4-phenyl-1,2,3,4-tetrahydropyrimidine-5-carboxylic acid ethyl ester

(2',3',4',6'-tetra-O-benzyl-β-D-galactopyranosyl)methyl azide