1-(2-bromo-4,5-dimethoxyphenyl)-8,9-dimethoxy-5,6-dihydropyrrolo[2,1-a]isoquinoline-2,3-dione

Base Information

Chemical Name:1-(2-bromo-4,5-dimethoxyphenyl)-8,9-dimethoxy-5,6-dihydropyrrolo[2,1-a]isoquinoline-2,3-dione
CAS No.:80041-82-3
Molecular Formula:C₂₂H₂₀BrNO₆
Molecular Weight:474.308
Hs Code.:

Synonyms:1-(2-Bromo-4,5-dimethoxy-phenyl)-8,9-dimethoxy-5,6-dihydro-pyrrolo[2,1-a]isoquinoline-2,3-dione

Suppliers and Price of 1-(2-bromo-4,5-dimethoxyphenyl)-8,9-dimethoxy-5,6-dihydropyrrolo[2,1-a]isoquinoline-2,3-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2-bromo-4,5-dimethoxyphenyl)-8,9-dimethoxy-5,6-dihydropyrrolo[2,1-a]isoquinoline-2,3-dione

Chemical Property:

Vapor Pressure:6.8E-15mmHg at 25°C

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 1-(2-bromo-4,5-dimethoxyphenyl)-8,9-dimethoxy-5,6-dihydropyrrolo[2,1-a]isoquinoline-2,3-dione

There total 1 articles about 1-(2-bromo-4,5-dimethoxyphenyl)-8,9-dimethoxy-5,6-dihydropyrrolo[2,1-a]isoquinoline-2,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 79-37-8
oxalyl dichloride

: 41823-67-0
1-(2'-bromo-4',5'-dimethoxybenzyl)-6,7-dimethoxy-3,4-dihydroisoquinoline

: 80041-82-3
1-(2-Bromo-4,5-dimethoxy-phenyl)-8,9-dimethoxy-5,6-dihydro-pyrrolo[2,1-a]isoquinoline-2,3-dione

Guidance literature:: With pyridine; for 2h; Ambient temperature;
DOI:10.1021/jo00342a028

Reference yield:

: 80041-82-3
1-(2-Bromo-4,5-dimethoxy-phenyl)-8,9-dimethoxy-5,6-dihydro-pyrrolo[2,1-a]isoquinoline-2,3-dione

: 5574-24-3
oxoglaucine

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / tert-butylamine / benzene / 24 h / Irradiation

2: 43 percent / 3percent aq. H₂O₂, 10percent aq. NaOH / dioxane / 3 h

With sodium hydroxide; dihydrogen peroxide; tert-butylamine; In 1,4-dioxane; benzene;
DOI:10.1021/jo00342a028