11-(tolylsulfonyl)-1-vinyl-5,6,11,11b-tetrahydro-3H-indolizino[8,7-b]indole

Base Information

Chemical Name:11-(tolylsulfonyl)-1-vinyl-5,6,11,11b-tetrahydro-3H-indolizino[8,7-b]indole
CAS No.:868847-24-9
Molecular Formula:C₂₃H₂₂N₂O₂S
Molecular Weight:390.506
Hs Code.:

Synonyms:11-(tolylsulfonyl)-1-vinyl-5,6,11,11b-tetrahydro-3H-indolizino[8,7-b]indole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 11-(tolylsulfonyl)-1-vinyl-5,6,11,11b-tetrahydro-3H-indolizino[8,7-b]indole

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Technology Process of 11-(tolylsulfonyl)-1-vinyl-5,6,11,11b-tetrahydro-3H-indolizino[8,7-b]indole

There total 10 articles about 11-(tolylsulfonyl)-1-vinyl-5,6,11,11b-tetrahydro-3H-indolizino[8,7-b]indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 868846-96-2
2-allyl-1-ethynyl-9-(tolylsulfonyl)-2,3,4,9-tetrahydro-1H-β-carboline

: 11-(tolylsulfonyl)-1-vinyl-6,11-dihydro-5H-indolizino[8,7-b]indole

: 868847-24-9
11-(tolylsulfonyl)-1-vinyl-5,6,11,11b-tetrahydro-3H-indolizino[8,7-b]indole

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In toluene; at 20 ℃;
DOI:10.1016/j.tetlet.2005.07.140

Reference yield: 41.0%

: 868846-96-2
2-allyl-1-ethynyl-9-(tolylsulfonyl)-2,3,4,9-tetrahydro-1H-β-carboline

: 762-42-5
dimethyl acetylenedicarboxylate

: 868847-24-9
11-(tolylsulfonyl)-1-vinyl-5,6,11,11b-tetrahydro-3H-indolizino[8,7-b]indole

: dimethyl (9E,11Z)-8-tosyl-11-vinyl-8,14-diazatetracyclo[12,2,2,0^1,9,0^2,7]octadeca-2,4,6,9,11,15-hexaene-15,16-dicarboxylate

Guidance literature:: 2-allyl-1-ethynyl-9-(tolylsulfonyl)-2,3,4,9-tetrahydro-1H-β-carboline; [Ru]-II catalyst; In toluene; for 96h;

dimethyl acetylenedicarboxylate; In toluene; at 60 ℃; for 5h; Further stages.;
DOI:10.1016/j.tetlet.2008.07.025

Reference yield: 8.0%

: 868846-96-2
2-allyl-1-ethynyl-9-(tolylsulfonyl)-2,3,4,9-tetrahydro-1H-β-carboline

: 762-42-5
dimethyl acetylenedicarboxylate

: 11-(tolylsulfonyl)-1-vinyl-6,11-dihydro-5H-indolizino[8,7-b]indole

: 868847-24-9
11-(tolylsulfonyl)-1-vinyl-5,6,11,11b-tetrahydro-3H-indolizino[8,7-b]indole

: dimethyl (9E,11Z)-8-tosyl-11-vinyl-8,14-diazatetracyclo[12.2.2.0(1,9).0(2,7)]octadeca-2,4,6,9,11,15-hexaene-15,16-dicarboxylate

Guidance literature:: 2-allyl-1-ethynyl-9-(tolylsulfonyl)-2,3,4,9-tetrahydro-1H-β-carboline; With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In toluene; for 96h;

dimethyl acetylenedicarboxylate; In toluene; at 60 ℃; for 5h;
DOI:10.1016/j.tet.2009.02.051