Technology Process of 5,10-dibenzyloxy-3,7,10-trioxacyclododecanone
There total 7 articles about 5,10-dibenzyloxy-3,7,10-trioxacyclododecanone which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Dess-Martin periodane;
In
dichloromethane;
at 20 ℃;
for 2h;
DOI:10.3987/COM-12-S(N)67
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium hydride / tetrahydrofuran / 2 h / 0 - 20 °C
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 - 20 °C
3: 3-chloro-benzenecarboperoxoic acid / chloroform / 24 h / 0 - 20 °C
4: boron trifluoride diethyl etherate / dichloromethane / 5 h / 0 - 20 °C
5: Dess-Martin periodane / dichloromethane / 2 h / 20 °C
With
boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; sodium hydride; Dess-Martin periodane; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane; chloroform;
DOI:10.3987/COM-12-S(N)67
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 3-chloro-benzenecarboperoxoic acid / chloroform / 24 h / 0 - 20 °C
2: boron trifluoride diethyl etherate / dichloromethane / 5 h / 0 - 20 °C
3: Dess-Martin periodane / dichloromethane / 2 h / 20 °C
With
boron trifluoride diethyl etherate; Dess-Martin periodane; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane; chloroform;
DOI:10.3987/COM-12-S(N)67
