1-Bromo-trans-2,3-diphenylcyclopropanecarboxyaldehyde

Base Information

Chemical Name:1-Bromo-trans-2,3-diphenylcyclopropanecarboxyaldehyde
CAS No.:84064-92-6
Molecular Formula:C₁₆H₁₃BrO
Molecular Weight:301.183
Hs Code.:

Synonyms:1-Bromo-trans-2,3-diphenylcyclopropanecarboxyaldehyde

Suppliers and Price of 1-Bromo-trans-2,3-diphenylcyclopropanecarboxyaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-Bromo-trans-2,3-diphenylcyclopropanecarboxyaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-Bromo-trans-2,3-diphenylcyclopropanecarboxyaldehyde

There total 1 articles about 1-Bromo-trans-2,3-diphenylcyclopropanecarboxyaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 33044-88-1
(3,3-dibromocyclopropane-1,2-diyl)dibenzene

: 109-94-4
formic acid ethyl ester

: 84064-92-6
1-Bromo-trans-2,3-diphenylcyclopropanecarboxyaldehyde

Guidance literature:: With n-butyllithium; In tetrahydrofuran; diethyl ether; 1) -110 degC, 5 min, 2) 4 h at low temperature before being warmed slowly to room temperature;
DOI:10.1021/jo00151a009

Reference yield: 57.0%

: 1779-49-3
Methyltriphenylphosphonium bromide

: 84064-92-6
1-Bromo-trans-2,3-diphenylcyclopropanecarboxyaldehyde

: 84064-87-9
C₁₇H₁₅Br

Guidance literature:: With n-butyllithium; In tetrahydrofuran; 1) room temperature, 2 h, 2) reflux, overnight;
DOI:10.1021/jo00151a009

Reference yield:

: 84064-92-6
1-Bromo-trans-2,3-diphenylcyclopropanecarboxyaldehyde

: 84064-93-7
1-Vinyl-trans-2,3-diphenylcyclopropane

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / n-BuLi / tetrahydrofuran / 1) room temperature, 2 h, 2) reflux, overnight

2: CH₃OD / tetrahydrofuran / -78 °C

With n-butyllithium; deuteromethanol; In tetrahydrofuran;
DOI:10.1021/jo00151a009