Technology Process of N,N-diisopropyl-2-phenylsulfonylpent-4-eneamide
There total 3 articles about N,N-diisopropyl-2-phenylsulfonylpent-4-eneamide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
N,N-diisopropyl-2-(phenylsulfonyl)acetamide;
With
sodium hydride;
In
dichloromethane; mineral oil;
at 20 ℃;
for 1h;
Inert atmosphere;
Allyl acetate;
With
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; (S)-(1,1'-binaphthalene)-2,2'-diylbis(diphenylphosphine);
In
dichloromethane; mineral oil;
at 20 ℃;
for 1.5h;
Inert atmosphere;
DOI:10.1007/s11172-008-0239-9
- Guidance literature:
-
N,N-diisopropyl-2-(phenylsulfonyl)acetamide;
With
sodium hydride;
In
dichloromethane; mineral oil;
at 20 ℃;
for 1h;
Inert atmosphere;
diallylcarbonate;
With
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; (S)-(1,1'-binaphthalene)-2,2'-diylbis(diphenylphosphine);
In
dichloromethane; mineral oil;
at 20 ℃;
for 1.5h;
Inert atmosphere;
DOI:10.1007/s11172-008-0239-9
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: dihydrogen peroxide / acetic acid / 20 - 100 °C
2.1: sodium hydride / dichloromethane; mineral oil / 1 h / 20 °C / Inert atmosphere
2.2: 1.5 h / 20 °C / Inert atmosphere
With
dihydrogen peroxide; sodium hydride;
In
dichloromethane; acetic acid; mineral oil;
DOI:10.1007/s11172-008-0239-9
