3,5-dimethoxybenzoyl isocyanate

Base Information

• Chemical Name: 3,5-dimethoxybenzoyl isocyanate
• CAS No.: 1061639-77-7
• Molecular Formula: C₁₀H₉NO₄
• Molecular Weight: 207.186

Synonyms:3,5-dimethoxybenzoyl isocyanate

Chemical Property of 3,5-dimethoxybenzoyl isocyanate

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 3,5-dimethoxybenzoyl isocyanate

There total 1 articles about 3,5-dimethoxybenzoyl isocyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

oxalyl dichloride (79-37-8) + 3,5-dimethoxybenzamide (17213-58-0) → 3,5-dimethoxybenzoyl isocyanate (1061639-77-7)

Guidance literature:

In 1,2-dichloro-ethane;

DOI:10.1021/jm800203e

Reference yield: 53.0%

6-amino-1,3-dihydro-indol-2-one (150544-04-0) + 3,5-dimethoxybenzoyl isocyanate (1061639-77-7) → N-(2-oxoindolin-6-ylcarbamoyl)-3,5-dimethoxybenzamide (1621584-42-6)

Guidance literature:

In acetonitrile; at 70 - 80 ℃;

DOI:10.1016/j.ejmech.2014.07.108

Reference yield:

3,5-dimethoxybenzoyl isocyanate (1061639-77-7) + 4″-epi-NH2-5-O-(tert-butyldimethylsilyl)doramectin → C66H98N2O17Si

Guidance literature:

With dmap; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1021/acs.jafc.0c00230

upstream raw materials:

oxalyl dichloride

3,5-dimethoxybenzamide

Downstream raw materials:

C₂₅H₂₄N₄O₆

C₃₂H₄₀N₄O₅S

C₂₅H₂₄N₄O₅S

C₂₃H₂₂N₄O₅S

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