trans-[4-(2-methanesulfonyl-vinyl)-cyclohexyl]-carbamic acid tert-butyl ester

Base Information

Chemical Name:trans-[4-(2-methanesulfonyl-vinyl)-cyclohexyl]-carbamic acid tert-butyl ester
CAS No.:1315499-03-6
Molecular Formula:C₁₄H₂₅NO₄S
Molecular Weight:303.423
Hs Code.:

Synonyms:trans-[4-(2-methanesulfonyl-vinyl)-cyclohexyl]-carbamic acid tert-butyl ester

Suppliers and Price of trans-[4-(2-methanesulfonyl-vinyl)-cyclohexyl]-carbamic acid tert-butyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of trans-[4-(2-methanesulfonyl-vinyl)-cyclohexyl]-carbamic acid tert-butyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of trans-[4-(2-methanesulfonyl-vinyl)-cyclohexyl]-carbamic acid tert-butyl ester

There total 2 articles about trans-[4-(2-methanesulfonyl-vinyl)-cyclohexyl]-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 181308-57-6
trans-(4-formyl-cyclohexyl)-carbamic acid tert-butyl ester

: 40137-11-9
diethyl methylsulfonylmethylphosphonate

: 1315499-03-6
trans-[4-(2-methanesulfonyl-vinyl)-cyclohexyl]-carbamic acid tert-butyl ester

Guidance literature:: diethyl methylsulfonylmethylphosphonate; With sodium hydride; In tetrahydrofuran; mineral oil; for 1h;

trans-(4-formyl-cyclohexyl)-carbamic acid tert-butyl ester; In tetrahydrofuran; mineral oil; for 2h;

Reference yield:

: 239074-29-4
trans (4-hydroxymethyl-cyclohexyl)-carbamic acid tert-butyl ester

: 1315499-03-6
trans-[4-(2-methanesulfonyl-vinyl)-cyclohexyl]-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine; sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 0 - 20 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h

2.2: 2 h

With sulfur trioxide pyridine complex; sodium hydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; mineral oil;