trans-[4-(2-methanesulfonyl-ethyl)-cyclohexyl]-carbamic acid tert-butyl ester

Base Information

Chemical Name:trans-[4-(2-methanesulfonyl-ethyl)-cyclohexyl]-carbamic acid tert-butyl ester
CAS No.:1315499-04-7
Molecular Formula:C₁₄H₂₇NO₄S
Molecular Weight:305.439
Hs Code.:

Synonyms:trans-[4-(2-methanesulfonyl-ethyl)-cyclohexyl]-carbamic acid tert-butyl ester

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Chemical Property of trans-[4-(2-methanesulfonyl-ethyl)-cyclohexyl]-carbamic acid tert-butyl ester

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Technology Process of trans-[4-(2-methanesulfonyl-ethyl)-cyclohexyl]-carbamic acid tert-butyl ester

There total 3 articles about trans-[4-(2-methanesulfonyl-ethyl)-cyclohexyl]-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1315499-03-6
trans-[4-(2-methanesulfonyl-vinyl)-cyclohexyl]-carbamic acid tert-butyl ester

: 1315499-04-7
trans-[4-(2-methanesulfonyl-ethyl)-cyclohexyl]-carbamic acid tert-butyl ester

Guidance literature:: With palladium 10% on activated carbon; ammonium formate; at 90 ℃; for 16.75h;

Reference yield:

: 239074-29-4
trans (4-hydroxymethyl-cyclohexyl)-carbamic acid tert-butyl ester

: 1315499-04-7
trans-[4-(2-methanesulfonyl-ethyl)-cyclohexyl]-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-ethyl-N,N-diisopropylamine; sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 0 - 20 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h

2.2: 2 h

3.1: ammonium formate; palladium 10% on activated carbon / 16.75 h / 90 °C

With palladium 10% on activated carbon; ammonium formate; sulfur trioxide pyridine complex; sodium hydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; mineral oil;

Reference yield:

: 181308-57-6
trans-(4-formyl-cyclohexyl)-carbamic acid tert-butyl ester

: 1315499-04-7
trans-[4-(2-methanesulfonyl-ethyl)-cyclohexyl]-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h

1.2: 2 h

2.1: ammonium formate; palladium 10% on activated carbon / 16.75 h / 90 °C

With palladium 10% on activated carbon; ammonium formate; sodium hydride; In tetrahydrofuran; mineral oil;