ethyl 2-(3-(2-fluorophenyl)-1-methyl-4-(trifluoromethyl)-1H-pyrazolo[3,4-b]pyridin-6-yloxy)acetate

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Chemical Name:ethyl 2-(3-(2-fluorophenyl)-1-methyl-4-(trifluoromethyl)-1H-pyrazolo[3,4-b]pyridin-6-yloxy)acetate
CAS No.:1312949-08-8
Molecular Formula:C₁₈H₁₅F₄N₃O₃
Molecular Weight:397.329
Hs Code.:

Synonyms:ethyl 2-(3-(2-fluorophenyl)-1-methyl-4-(trifluoromethyl)-1H-pyrazolo[3,4-b]pyridin-6-yloxy)acetate

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Chemical Property of ethyl 2-(3-(2-fluorophenyl)-1-methyl-4-(trifluoromethyl)-1H-pyrazolo[3,4-b]pyridin-6-yloxy)acetate

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Technology Process of ethyl 2-(3-(2-fluorophenyl)-1-methyl-4-(trifluoromethyl)-1H-pyrazolo[3,4-b]pyridin-6-yloxy)acetate

There total 3 articles about ethyl 2-(3-(2-fluorophenyl)-1-methyl-4-(trifluoromethyl)-1H-pyrazolo[3,4-b]pyridin-6-yloxy)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1312949-07-7
3-(2-fluorophenyl)-1-methyl-4-(trifluoromethyl)-1H-pyrazolo-[3,4-b]pyridin-6(7H)-one

: 105-36-2
ethyl bromoacetate

: 1312949-08-8
ethyl 2-(3-(2-fluorophenyl)-1-methyl-4-(trifluoromethyl)-1H-pyrazolo[3,4-b]pyridin-6-yloxy)acetate

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 3h; Inert atmosphere;

Reference yield:

: 31915-26-1
3-(2-fluorophenyl)-3-oxo-propanenitrile

: 1312949-08-8
ethyl 2-(3-(2-fluorophenyl)-1-methyl-4-(trifluoromethyl)-1H-pyrazolo[3,4-b]pyridin-6-yloxy)acetate

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 7 h / 120 °C

2: acetic acid / 1.5 h / 150 °C / microwave irradiation

3: sodium hydride / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere

With sodium hydride; acetic acid; In methanol; N,N-dimethyl-formamide;

Reference yield:

: 1012879-56-9
5-amino-3-(2-fluorophenyl)-1-methylpyrazole

: 1312949-08-8
ethyl 2-(3-(2-fluorophenyl)-1-methyl-4-(trifluoromethyl)-1H-pyrazolo[3,4-b]pyridin-6-yloxy)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / 1.5 h / 150 °C / microwave irradiation

2: sodium hydride / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere

With sodium hydride; acetic acid; In N,N-dimethyl-formamide;