Technology Process of C25H22FN5O4S
There total 5 articles about C25H22FN5O4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane;
at 20 ℃;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 90 °C / Neat (no solvent); Inert atmosphere
2.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0.5 h / 20 °C / Inert atmosphere
2.2: 0.5 h / Inert atmosphere
3.1: sodium chlorite; sodium dihydrogenphosphate; 2-Methyl-1-butene / tert-butyl alcohol / 0.67 h / 20 °C / Inert atmosphere
4.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C / Inert atmosphere
With
dmap; sodium chlorite; sodium dihydrogenphosphate; sodium hydrogencarbonate; Dess-Martin periodane; 2-Methyl-1-butene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane; tert-butyl alcohol;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium nitrite / water / 0 °C / Inert atmosphere
1.2: 0 - 20 °C / Inert atmosphere
1.3: Inert atmosphere
2.1: 90 °C / Neat (no solvent); Inert atmosphere
3.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0.5 h / 20 °C / Inert atmosphere
3.2: 0.5 h / Inert atmosphere
4.1: sodium chlorite; sodium dihydrogenphosphate; 2-Methyl-1-butene / tert-butyl alcohol / 0.67 h / 20 °C / Inert atmosphere
5.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C / Inert atmosphere
With
dmap; sodium chlorite; sodium dihydrogenphosphate; sodium hydrogencarbonate; Dess-Martin periodane; 2-Methyl-1-butene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium nitrite;
In
dichloromethane; water; tert-butyl alcohol;