2-(((tert-butyl)diphenylsilyloxy)methyl)-3,3-dimethyl-1-vinylcyclohexanol

Base Information

Chemical Name:2-(((tert-butyl)diphenylsilyloxy)methyl)-3,3-dimethyl-1-vinylcyclohexanol
CAS No.:1332864-63-7
Molecular Formula:C₂₇H₃₈O₂Si
Molecular Weight:422.683
Hs Code.:

Synonyms:2-(((tert-butyl)diphenylsilyloxy)methyl)-3,3-dimethyl-1-vinylcyclohexanol

Suppliers and Price of 2-(((tert-butyl)diphenylsilyloxy)methyl)-3,3-dimethyl-1-vinylcyclohexanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(((tert-butyl)diphenylsilyloxy)methyl)-3,3-dimethyl-1-vinylcyclohexanol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-(((tert-butyl)diphenylsilyloxy)methyl)-3,3-dimethyl-1-vinylcyclohexanol

There total 3 articles about 2-(((tert-butyl)diphenylsilyloxy)methyl)-3,3-dimethyl-1-vinylcyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1332864-62-6
2-(((tert-butyldiphenylsilyl)oxy)methyl)-3,3-dimethylcyclohexan-1-one

: 1826-67-1
vinyl magnesium bromide

: 1332864-63-7
2-(((tert-butyl)diphenylsilyloxy)methyl)-3,3-dimethyl-1-vinylcyclohexanol

Guidance literature:: In tetrahydrofuran; at 0 ℃; Inert atmosphere;
DOI:10.1021/ja2066219

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1332864-63-7
2-(((tert-butyl)diphenylsilyloxy)methyl)-3,3-dimethyl-1-vinylcyclohexanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 0 - 30 °C / Inert atmosphere

1.2: 0 °C / Inert atmosphere

2.1: tetrahydrofuran / 0 °C / Inert atmosphere

With 1H-imidazole; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/ja2066219

Reference yield:

: 99182-73-7
2-(hydroxymethyl)-3,3-dimethylcyclohexan-1-one

: 1332864-63-7
2-(((tert-butyl)diphenylsilyloxy)methyl)-3,3-dimethyl-1-vinylcyclohexanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 0 - 30 °C / Inert atmosphere

1.2: 0 °C / Inert atmosphere

2.1: tetrahydrofuran / 0 °C / Inert atmosphere

With 1H-imidazole; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/ja2066219