Technology Process of C23H36N2O2
There total 7 articles about C23H36N2O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
for 0.5h;
Cooling with ice;
DOI:10.1016/j.cclet.2016.03.006
- Guidance literature:
-
Multi-step reaction with 5 steps
1: water; potassium hydroxide / 9 h / Reflux
2: methanol; Petroleum ether
3: potassium carbonate / dichloromethane / 20 °C
4: 3-methyl-phenol / 80 °C
5: lithium aluminium tetrahydride / tetrahydrofuran / Reflux
With
lithium aluminium tetrahydride; water; potassium carbonate; 3-methyl-phenol; potassium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; Petroleum ether;
DOI:10.1016/j.bmcl.2011.06.071
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrogenchloride / 2 h / Reflux
2: potassium carbonate / acetonitrile / 8 h / 20 °C
3: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / Cooling with ice
With
hydrogenchloride; lithium aluminium tetrahydride; potassium carbonate;
In
tetrahydrofuran; acetonitrile;
DOI:10.1016/j.cclet.2016.03.006