(±)-ethyl 2-oxo-4-phenyl-6-(3,4,5-trimethoxyphenyl)cyclohex-3-encarboxylate

Base Information

Chemical Name:(±)-ethyl 2-oxo-4-phenyl-6-(3,4,5-trimethoxyphenyl)cyclohex-3-encarboxylate
CAS No.:1251828-10-0
Molecular Formula:C₂₄H₂₆O₆
Molecular Weight:410.467
Hs Code.:

Synonyms:(±)-ethyl 2-oxo-4-phenyl-6-(3,4,5-trimethoxyphenyl)cyclohex-3-encarboxylate

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Chemical Property of (±)-ethyl 2-oxo-4-phenyl-6-(3,4,5-trimethoxyphenyl)cyclohex-3-encarboxylate

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Technology Process of (±)-ethyl 2-oxo-4-phenyl-6-(3,4,5-trimethoxyphenyl)cyclohex-3-encarboxylate

There total 5 articles about (±)-ethyl 2-oxo-4-phenyl-6-(3,4,5-trimethoxyphenyl)cyclohex-3-encarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 127034-55-3
1-phenyl-3-(3,4,5-trimethoxyphenyl)-trans-prop-2-en-1-one

: 141-97-9
ethyl acetoacetate

: 1251828-10-0
(±)-ethyl 2-oxo-4-phenyl-6-(3,4,5-trimethoxyphenyl)cyclohex-3-encarboxylate

Guidance literature:: With silica gel; potassium carbonate; Microwave irradiation;
DOI:10.1016/j.ejmech.2012.10.038

Reference yield: 59.0%

: 127034-55-3,60246-63-1
3,4,5-trimethoxychalcone

: 141-97-9
ethyl acetoacetate

: 1251828-10-0
(±)-ethyl 2-oxo-4-phenyl-6-(3,4,5-trimethoxyphenyl)cyclohex-3-encarboxylate

Guidance literature:: ethyl acetoacetate; With sodium ethanolate; at 20 ℃; for 1h;

3,4,5-trimethoxychalcone; for 5h; Reflux;
DOI:10.2174/1573406411309050012

Reference yield:

: 98-86-2
acetophenone

: 1251828-10-0
(±)-ethyl 2-oxo-4-phenyl-6-(3,4,5-trimethoxyphenyl)cyclohex-3-encarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / ethanol / 12 h / 20 °C

2.1: sodium ethanolate / 1 h / 20 °C

2.2: 5 h / Reflux

With sodium ethanolate; sodium hydroxide; In ethanol;
DOI:10.2174/1573406411309050012