(Z)-O-acetylbenzohydroximoyl chloride

Base Information

• Chemical Name: (Z)-O-acetylbenzohydroximoyl chloride
• CAS No.: 90690-86-1
• Molecular Formula: C₉H₈ClNO₂
• Molecular Weight: 197.621
• Mol file: 90690-86-1.mol

Synonyms:(Z)-O-acetylbenzohydroximoyl chloride

Chemical Property of (Z)-O-acetylbenzohydroximoyl chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (Z)-O-acetylbenzohydroximoyl chloride

There total 2 articles about (Z)-O-acetylbenzohydroximoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

acetyl chloride (75-36-5) + phenylhydroxamoyl chloride (934-16-7) → (Z)-O-acetylbenzohydroximoyl chloride (90690-86-1)

Guidance literature:

With pyridine; In benzene; for 1h; Ambient temperature;

Reference yield:

Benzaldoxime (932-90-1) → (Z)-O-acetylbenzohydroximoyl chloride (90690-86-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 70 percent / chlorine / CHCl₃ / 0.5 h / 0 °C

2: 90 percent / pyridine / benzene / 1 h / Ambient temperature

With pyridine; chlorine; In chloroform; benzene;

Reference yield:

(Z)-O-acetylbenzohydroximoyl chloride (90690-86-1) → Acetic acid 5-phenyl-tetrazol-1-yl ester

Guidance literature:

Multi-step reaction with 2 steps

1: NaN₃ / acetone; H₂O / 25 °C

2: AcCl / benzene / 72 h / 80 °C

With sodium azide; acetyl chloride; In water; acetone; benzene;

DOI:10.1039/c39840000913

upstream raw materials:

acetyl chloride

phenylhydroxamoyl chloride

Benzaldoxime

Downstream raw materials:

C₉H₈N₄O₂

α-chloro-o-acetylbenzaldoxime