N-(naphthalene-2-sulfonyl)-N'-(p-toluenesulfonyl)bis(3-aminopropyl)cyclohexylmethylamine

Base Information

Chemical Name:N-(naphthalene-2-sulfonyl)-N'-(p-toluenesulfonyl)bis(3-aminopropyl)cyclohexylmethylamine
CAS No.:1322645-15-7
Molecular Formula:C₃₀H₄₁N₃O₄S₂
Molecular Weight:571.805
Hs Code.:

Synonyms:N-(naphthalene-2-sulfonyl)-N'-(p-toluenesulfonyl)bis(3-aminopropyl)cyclohexylmethylamine

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Chemical Property of N-(naphthalene-2-sulfonyl)-N'-(p-toluenesulfonyl)bis(3-aminopropyl)cyclohexylmethylamine

Chemical Property:

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Technology Process of N-(naphthalene-2-sulfonyl)-N'-(p-toluenesulfonyl)bis(3-aminopropyl)cyclohexylmethylamine

There total 8 articles about N-(naphthalene-2-sulfonyl)-N'-(p-toluenesulfonyl)bis(3-aminopropyl)cyclohexylmethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1322645-94-2
N-(naphthalene-2-sulfonyl)-N'-(p-toluenesulfonyl)bis(3-aminopropyl)cyclohexylmethylamine hydrochloride

: 1322645-15-7
N-(naphthalene-2-sulfonyl)-N'-(p-toluenesulfonyl)bis(3-aminopropyl)cyclohexylmethylamine

Guidance literature:: With sodium chloride; sodium hydroxide; In dichloromethane; water; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1021/jm2002603

Reference yield:

: 1322644-99-4
N-(p-toluenesulfonamidopropyl)cyclohexylmethylamine

: 1322645-15-7
N-(naphthalene-2-sulfonyl)-N'-(p-toluenesulfonyl)bis(3-aminopropyl)cyclohexylmethylamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium carbonate / acetonitrile / 48 h / Inert atmosphere; Reflux

2.1: hydrazine hydrate / ethanol / 3 h / Inert atmosphere; Reflux

2.2: 1.5 h / Inert atmosphere

3.1: sodium carbonate; sodium chloride / dichloromethane; water / 24 h / 20 °C / Inert atmosphere

3.2: 4 h / 20 °C / Inert atmosphere

4.1: sodium chloride; sodium hydroxide / dichloromethane; water / 4 h / 20 °C / Inert atmosphere

With sodium carbonate; hydrazine hydrate; sodium chloride; sodium hydroxide; In ethanol; dichloromethane; water; acetonitrile;
DOI:10.1021/jm2002603

Reference yield:

: C₁₇H₂₆N₂O₂S

: 1322645-15-7
N-(naphthalene-2-sulfonyl)-N'-(p-toluenesulfonyl)bis(3-aminopropyl)cyclohexylmethylamine

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium tetrahydroborate / ethanol / 12 h / 20 °C / Inert atmosphere

2.1: sodium carbonate / acetonitrile / 48 h / Inert atmosphere; Reflux

3.1: hydrazine hydrate / ethanol / 3 h / Inert atmosphere; Reflux

3.2: 1.5 h / Inert atmosphere

4.1: sodium carbonate; sodium chloride / dichloromethane; water / 24 h / 20 °C / Inert atmosphere

4.2: 4 h / 20 °C / Inert atmosphere

5.1: sodium chloride; sodium hydroxide / dichloromethane; water / 4 h / 20 °C / Inert atmosphere

With sodium tetrahydroborate; sodium carbonate; hydrazine hydrate; sodium chloride; sodium hydroxide; In ethanol; dichloromethane; water; acetonitrile;
DOI:10.1021/jm2002603