(2''S,3''R,6''S)-N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyl)-N-[2'-(2''-methoxy-6''-oxymethyl-3'',6''-dihydro-2''H-pyran-3''-yloxymethyl)-allyl]-4'''-methylbenzenesulfonamide

Base Information

• Chemical Name: (2''S,3''R,6''S)-N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyl)-N-[2'-(2''-methoxy-6''-oxymethyl-3'',6''-dihydro-2''H-pyran-3''-yloxymethyl)-allyl]-4'''-methylbenzenesulfonamide
• CAS No.: 1120367-34-1
• Molecular Formula: C₂₈H₂₈F₁₇NO₆S
• Molecular Weight: 829.572

Synonyms:(2''S,3''R,6''S)-N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyl)-N-[2'-(2''-methoxy-6''-oxymethyl-3'',6''-dihydro-2''H-pyran-3''-yloxymethyl)-allyl]-4'''-methylbenzenesulfonamide

Chemical Property of (2''S,3''R,6''S)-N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyl)-N-[2'-(2''-methoxy-6''-oxymethyl-3'',6''-dihydro-2''H-pyran-3''-yloxymethyl)-allyl]-4'''-methylbenzenesulfonamide

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Technology Process of (2''S,3''R,6''S)-N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyl)-N-[2'-(2''-methoxy-6''-oxymethyl-3'',6''-dihydro-2''H-pyran-3''-yloxymethyl)-allyl]-4'''-methylbenzenesulfonamide

There total 2 articles about (2''S,3''R,6''S)-N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyl)-N-[2'-(2''-methoxy-6''-oxymethyl-3'',6''-dihydro-2''H-pyran-3''-yloxymethyl)-allyl]-4'''-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(2''S,3''R,6''S)-N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyl)-N-[2'-(2''S-methoxy-6''S-formoxymethyl-3'',6''-dihydro-2''H-pyran-3''-yloxymethyl)-allyl]-4'''-methylbenzenesulfonamide (1120367-42-1) → (2''S,3''R,6''S)-N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyl)-N-[2'-(2''-methoxy-6''-oxymethyl-3'',6''-dihydro-2''H-pyran-3''-yloxymethyl)-allyl]-4'''-methylbenzenesulfonamide (1120367-34-1)

Guidance literature:

With methanol; sodium methylate; Inert atmosphere;

DOI:10.1021/ol802848j

Reference yield: 26.0%

formic acid (64-18-6) + (2''S,3''R,6''S)-N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyl)-N-[2'-(2''-methoxy-6''-trityloxymethyl-3'',6''-dihydro-2''H-pyran-3''-yloxymethyl)-allyl]-4'''-methylbenzenesulfonamide (1120367-41-0) → (2''S,3''R,6''S)-N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyl)-N-[2'-(2''-methoxy-6''-oxymethyl-3'',6''-dihydro-2''H-pyran-3''-yloxymethyl)-allyl]-4'''-methylbenzenesulfonamide (1120367-34-1) + (2''S,3''R,6''S)-N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyl)-N-[2'-(2''S-methoxy-6''S-formoxymethyl-3'',6''-dihydro-2''H-pyran-3''-yloxymethyl)-allyl]-4'''-methylbenzenesulfonamide (1120367-42-1)

Guidance literature:

With triethylsilane; In tetrahydrofuran; water; at 20 ℃; for 2h;

DOI:10.1021/ol802848j

Reference yield: 89.0%

pent-4-enoic acid (591-80-0) + (2''S,3''R,6''S)-N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyl)-N-[2'-(2''-methoxy-6''-oxymethyl-3'',6''-dihydro-2''H-pyran-3''-yloxymethyl)-allyl]-4'''-methylbenzenesulfonamide (1120367-34-1) → [(2S,5R,6S)-5-{2-[{N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-4-methylphenylsulfonamido}methyl]allyloxy}-6-methoxy-5,6-dihydro-2H-pyran-2-yl]methyl pent-4'-enoate (1120367-81-8)

Guidance literature:

With dmap; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; for 18h; Inert atmosphere;

DOI:10.1021/ol802848j

upstream raw materials:

formic acid

(2''S,3''R,6''S)-N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyl)-N-[2'-(2''-methoxy-6''-trityloxymethyl-3'',6''-dihydro-2''H-pyran-3''-yloxymethyl)-allyl]-4'''-methylbenzenesulfonamide

(2''S,3''R,6''S)-N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-decyl)-N-[2'-(2''S-methoxy-6''S-formoxymethyl-3'',6''-dihydro-2''H-pyran-3''-yloxymethyl)-allyl]-4'''-methylbenzenesulfonamide

Downstream raw materials:

N-(2-{[(2S,3R,6S)-6-[(diisopropyl((R)-1'-phenylallyloxy)silyloxy)methyl]-2-methoxy-3,6-dihydro-2H-pyran-3-yloxy]methyl}allyl)-N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-4-methylbenzenesulfonamide

N-(2-{[(2S,3R,6S)-6-[(diisopropyl((S)-pent-4'-en-2'-yloxy)silyloxy)methyl]-2-methoxy-3,6-dihydro-2H-pyran-3-yloxy]methyl}allyl)-N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-4-methylbenzenesulfonamide

N-(2-{[(2S,3R,6S)-6-[(diisopropyl((S)-pent-4'-en-2'-yloxy)silyloxy)methyl]-2-methoxy-3,6-dihydro-2H-pyran-3-yloxy]methyl}allyl)-N-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-4-methylbenzenesulfonamide

N-[4-(allyloxy)but-2-yn-1-yl]-N-{[(2'S,5'R,6'S)-5'-{2-[(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)-4-methylphenylsulfonamido]methyl}allyloxy-6'-methoxy-5',6'-dihydro-2H-pyran-2'-yl]methyl}-2-nitrobenzenesulfonamide

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