N-[6-Chloro-4-(1-hydroxy-4-methyl-5-pyridin-3-yl-1H-imidazol-2-yl)-3-methoxy-2-nitro-phenyl]-acetamide

Base Information

Chemical Name:N-[6-Chloro-4-(1-hydroxy-4-methyl-5-pyridin-3-yl-1H-imidazol-2-yl)-3-methoxy-2-nitro-phenyl]-acetamide
CAS No.:1027193-54-9
Molecular Formula:C₁₈H₁₆ClN₅O₅
Molecular Weight:417.809
Hs Code.:

Synonyms:N-[6-Chloro-4-(1-hydroxy-4-methyl-5-pyridin-3-yl-1H-imidazol-2-yl)-3-methoxy-2-nitro-phenyl]-acetamide

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Chemical Property of N-[6-Chloro-4-(1-hydroxy-4-methyl-5-pyridin-3-yl-1H-imidazol-2-yl)-3-methoxy-2-nitro-phenyl]-acetamide

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Technology Process of N-[6-Chloro-4-(1-hydroxy-4-methyl-5-pyridin-3-yl-1H-imidazol-2-yl)-3-methoxy-2-nitro-phenyl]-acetamide

There total 4 articles about N-[6-Chloro-4-(1-hydroxy-4-methyl-5-pyridin-3-yl-1H-imidazol-2-yl)-3-methoxy-2-nitro-phenyl]-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65882-96-4
1-hydroxyimino-1-(3-pyridyl)-2-propanone

: 156601-87-5
N-(6-Chloro-4-formyl-3-methoxy-2-nitro-phenyl)-acetamide

: 1027193-54-9
N-[6-Chloro-4-(1-hydroxy-4-methyl-5-pyridin-3-yl-1H-imidazol-2-yl)-3-methoxy-2-nitro-phenyl]-acetamide

Guidance literature:: With ammonium acetate; In acetic acid; at 100 ℃; for 0.25h;
DOI:10.1248/cpb.42.560

Reference yield:

: 4093-31-6
methyl 2-methoxy 4-acetamido 5-chloro benzoate

: 1027193-54-9
N-[6-Chloro-4-(1-hydroxy-4-methyl-5-pyridin-3-yl-1H-imidazol-2-yl)-3-methoxy-2-nitro-phenyl]-acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: 93.8 percent / HNO₃ fuming / 0.17 h / -35 - -30 °C

2: LiAlH₄ / tetrahydrofuran / 2 h / -30 °C

3: 84 percent / MnO₂ / ethyl acetate / 6 h / Heating

4: ammonium acetate / acetic acid / 0.25 h / 100 °C

With ammonium acetate; manganese(IV) oxide; lithium aluminium tetrahydride; nitric acid; In tetrahydrofuran; acetic acid; ethyl acetate;
DOI:10.1248/cpb.42.560

Reference yield:

: 1027594-75-7
N-(6-Chloro-4-hydroxymethyl-3-methoxy-2-nitro-phenyl)-acetamide

: 1027193-54-9
N-[6-Chloro-4-(1-hydroxy-4-methyl-5-pyridin-3-yl-1H-imidazol-2-yl)-3-methoxy-2-nitro-phenyl]-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / MnO₂ / ethyl acetate / 6 h / Heating

2: ammonium acetate / acetic acid / 0.25 h / 100 °C

With ammonium acetate; manganese(IV) oxide; In acetic acid; ethyl acetate;
DOI:10.1248/cpb.42.560