C₃₃H₃₂FNO₄

Base Information

Chemical Name:C₃₃H₃₂FNO₄
CAS No.:1429060-38-7
Molecular Formula:C₃₃H₃₂FNO₄
Molecular Weight:525.62
Hs Code.:

C<sub>33</sub>H<sub>32</sub>FNO<sub>4</sub>

Synonyms:C₃₃H₃₂FNO₄

Suppliers and Price of C₃₃H₃₂FNO₄

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Chemical Property of C₃₃H₃₂FNO₄

Chemical Property:

Purity/Quality:

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Technology Process of C₃₃H₃₂FNO₄

There total 9 articles about C₃₃H₃₂FNO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1441636-18-5
C₄₃H₄₁FN₂O₅

: 1429060-38-7
C₃₃H₃₂FNO₄

Guidance literature:: With lithium hydroxide monohydrate; dihydrogen peroxide; In tetrahydrofuran; water; at 0 ℃; for 3.5h; Inert atmosphere;
DOI:10.1016/j.bmc.2013.02.003

Reference yield:

: 176047-66-8
benzyl 2-hydroxy-5-formylbenzoate

: 1429060-38-7
C₃₃H₃₂FNO₄

Guidance literature:: Multi-step reaction with 9 steps

1: potassium carbonate / N,N-dimethyl-formamide / 60 °C

2: sodium tetrahydroborate / ethanol / 2 h / 20 °C

3: phosphorus tribromide / diethyl ether / 1.5 h / 0 °C

4: lithium hexamethyldisilazane / tetrahydrofuran / 2 h / -50 - 0 °C

5: palladium 10% on activated carbon; hydrogen / ethyl acetate / 3 h / 20 °C

6: borane-THF / tetrahydrofuran / 0 °C

7: manganese(IV) oxide / dichloromethane / 20 °C

8: triethylsilane; trifluoroacetic acid / toluene / 48 h / Reflux

9: lithium hydroxide monohydrate; dihydrogen peroxide / tetrahydrofuran; water / 3.5 h / 0 °C / Inert atmosphere

With triethylsilane; manganese(IV) oxide; sodium tetrahydroborate; borane-THF; lithium hydroxide monohydrate; palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; phosphorus tribromide; potassium carbonate; trifluoroacetic acid; lithium hexamethyldisilazane; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmc.2013.02.003

Reference yield:

: 616-76-2
2-hydroxy-5-formylbenzoic acid

: 1429060-38-7
C₃₃H₃₂FNO₄

Guidance literature:: Multi-step reaction with 10 steps

1: potassium hydrogencarbonate / N,N-dimethyl-formamide / 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 60 °C

3: sodium tetrahydroborate / ethanol / 2 h / 20 °C

4: phosphorus tribromide / diethyl ether / 1.5 h / 0 °C

5: lithium hexamethyldisilazane / tetrahydrofuran / 2 h / -50 - 0 °C

6: palladium 10% on activated carbon; hydrogen / ethyl acetate / 3 h / 20 °C

7: borane-THF / tetrahydrofuran / 0 °C

8: manganese(IV) oxide / dichloromethane / 20 °C

9: triethylsilane; trifluoroacetic acid / toluene / 48 h / Reflux

10: lithium hydroxide monohydrate; dihydrogen peroxide / tetrahydrofuran; water / 3.5 h / 0 °C / Inert atmosphere

With triethylsilane; manganese(IV) oxide; sodium tetrahydroborate; borane-THF; lithium hydroxide monohydrate; palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; phosphorus tribromide; potassium carbonate; potassium hydrogencarbonate; trifluoroacetic acid; lithium hexamethyldisilazane; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmc.2013.02.003