10-methoxy-9-(phenylmethoxy)-5,6,7,8,13,13a-hexahydro-2H-1,3-dioxolano[4,5-g]isoquinolino[3,2-a]isoquinoline

Base Information

Chemical Name:10-methoxy-9-(phenylmethoxy)-5,6,7,8,13,13a-hexahydro-2H-1,3-dioxolano[4,5-g]isoquinolino[3,2-a]isoquinoline
CAS No.:1095271-37-6
Molecular Formula:C₂₆H₂₅NO₄
Molecular Weight:415.489
Hs Code.:

Synonyms:10-methoxy-9-(phenylmethoxy)-5,6,7,8,13,13a-hexahydro-2H-1,3-dioxolano[4,5-g]isoquinolino[3,2-a]isoquinoline

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Chemical Property of 10-methoxy-9-(phenylmethoxy)-5,6,7,8,13,13a-hexahydro-2H-1,3-dioxolano[4,5-g]isoquinolino[3,2-a]isoquinoline

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Technology Process of 10-methoxy-9-(phenylmethoxy)-5,6,7,8,13,13a-hexahydro-2H-1,3-dioxolano[4,5-g]isoquinolino[3,2-a]isoquinoline

There total 4 articles about 10-methoxy-9-(phenylmethoxy)-5,6,7,8,13,13a-hexahydro-2H-1,3-dioxolano[4,5-g]isoquinolino[3,2-a]isoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 17388-17-9
(+/-)-nandinine

: 1095271-37-6
10-methoxy-9-(phenylmethoxy)-5,6,7,8,13,13a-hexahydro-2H-1,3-dioxolano[4,5-g]isoquinolino[3,2-a]isoquinoline

Guidance literature:: With potassium carbonate; In acetone; at 70 ℃; for 3h;

Reference yield:

: 633-65-8
berberine chloride

: 1095271-37-6
10-methoxy-9-(phenylmethoxy)-5,6,7,8,13,13a-hexahydro-2H-1,3-dioxolano[4,5-g]isoquinolino[3,2-a]isoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: 0.5 h / 190 °C

2: sodium tetrahydroborate; methanol / 0.25 h / 60 °C

3: potassium carbonate / 3 h / 70 °C

With methanol; sodium tetrahydroborate; potassium carbonate;

Reference yield:

: 15401-69-1
berberrubine chloride

: 1095271-37-6
10-methoxy-9-(phenylmethoxy)-5,6,7,8,13,13a-hexahydro-2H-1,3-dioxolano[4,5-g]isoquinolino[3,2-a]isoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate; methanol / 0.25 h / 60 °C

2: potassium carbonate / 3 h / 70 °C

With methanol; sodium tetrahydroborate; potassium carbonate;