2,3'-anhydro-3-(5-O-trityl-2,3-dideoxy-β-D-threo-pentofuranosyl)-5-iodouracil

Base Information

Chemical Name:2,3'-anhydro-3-(5-O-trityl-2,3-dideoxy-β-D-threo-pentofuranosyl)-5-iodouracil
CAS No.:101039-83-2
Molecular Formula:C₂₈H₂₃IN₂O₄
Molecular Weight:578.406
Hs Code.:

Synonyms:2,3'-anhydro-3-(5-O-trityl-2,3-dideoxy-β-D-threo-pentofuranosyl)-5-iodouracil

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Chemical Property of 2,3'-anhydro-3-(5-O-trityl-2,3-dideoxy-β-D-threo-pentofuranosyl)-5-iodouracil

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Technology Process of 2,3'-anhydro-3-(5-O-trityl-2,3-dideoxy-β-D-threo-pentofuranosyl)-5-iodouracil

There total 3 articles about 2,3'-anhydro-3-(5-O-trityl-2,3-dideoxy-β-D-threo-pentofuranosyl)-5-iodouracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 101039-82-1
5-iodo-3'-O-mesyl-5'-O-trityl-2'-deoxyuridine

: 101039-83-2
2,3'-anhydro-3-(5-O-trityl-2,3-dideoxy-β-D-threo-pentofuranosyl)-5-iodouracil

: 101039-85-4
2,3'-anydro-5-iodo-5'-O-trityl-2'-deoxyuridine

: 1-(3-azido-2,3-dideoxy-5-O-trityl-β-D-threo-pentofuranosyl)-5-iodouracil

: 87190-83-8
1-(3-azido-2,3-dideoxy-5-O-trityl-β-D-erythro-pentofuranosyl)-5-iodouracil

Guidance literature:: With lithium azide; In N,N-dimethyl-formamide; at 100 ℃; for 5h;

Reference yield: 24.0%

: 101039-85-4
2,3'-anydro-5-iodo-5'-O-trityl-2'-deoxyuridine

: 101039-83-2
2,3'-anhydro-3-(5-O-trityl-2,3-dideoxy-β-D-threo-pentofuranosyl)-5-iodouracil

Guidance literature:: With toluene-4-sulfonic acid; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 150 ℃; for 2.5h;

Reference yield:

: 101039-82-1
5-iodo-3'-O-mesyl-5'-O-trityl-2'-deoxyuridine

: 101039-83-2
2,3'-anhydro-3-(5-O-trityl-2,3-dideoxy-β-D-threo-pentofuranosyl)-5-iodouracil

Guidance literature:: Multi-step reaction with 2 steps

1: 13 percent / LiN₃ / dimethylformamide / 5 h / 100 °C

2: 24 percent / p-toluenesulfonic acid / hexamethylphosphoric acid triamide / 2.5 h / 150 °C

With lithium azide; toluene-4-sulfonic acid; In N,N,N,N,N,N-hexamethylphosphoric triamide; N,N-dimethyl-formamide;