allyl 2-O-(2-(azidomethyl)benzoyl)-4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranoside

Base Information

Chemical Name:allyl 2-O-(2-(azidomethyl)benzoyl)-4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranoside
CAS No.:1349064-78-3
Molecular Formula:C₃₂H₃₅N₃O₇
Molecular Weight:573.646
Hs Code.:

Synonyms:allyl 2-O-(2-(azidomethyl)benzoyl)-4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of allyl 2-O-(2-(azidomethyl)benzoyl)-4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranoside

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Technology Process of allyl 2-O-(2-(azidomethyl)benzoyl)-4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranoside

There total 11 articles about allyl 2-O-(2-(azidomethyl)benzoyl)-4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 144174-52-7
allyl 4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranoside

: 289712-57-8
2-(azidomethyl)benzoic acid

: 1349064-78-3
allyl 2-O-(2-(azidomethyl)benzoyl)-4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranoside

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 4h; Inert atmosphere; Reflux;

Reference yield: 91.0%

: 144174-52-7
allyl 4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranoside

: 289712-58-9
2-(azidomethyl)benzoyl chloride

: 1349064-78-3
allyl 2-O-(2-(azidomethyl)benzoyl)-4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranoside

Guidance literature:: With dmap; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

Reference yield:

: 329781-57-9
methyl 2-(azidomethyl) benzoate

: 1349064-78-3
allyl 2-O-(2-(azidomethyl)benzoyl)-4-O-benzyl-3-O-para-methoxybenzyl-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide; water / methanol / 2 h / 20 °C

2: thionyl chloride / 1 h / Inert atmosphere; Reflux

3: dmap / dichloromethane / 1 h / 20 °C / Inert atmosphere

With dmap; thionyl chloride; water; sodium hydroxide; In methanol; dichloromethane;