N-Benzyl-4-(3,4-dihydro-2,6-naphthyridin-2(1H)-yl)-N-methylcyclohexanamine

Base Information

Chemical Name:N-Benzyl-4-(3,4-dihydro-2,6-naphthyridin-2(1H)-yl)-N-methylcyclohexanamine
CAS No.:1365156-20-2
Molecular Formula:C₂₂H₂₉N₃
Molecular Weight:335.492
Hs Code.:

Synonyms:N-Benzyl-4-(3,4-dihydro-2,6-naphthyridin-2(1H)-yl)-N-methylcyclohexanamine

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Chemical Property of N-Benzyl-4-(3,4-dihydro-2,6-naphthyridin-2(1H)-yl)-N-methylcyclohexanamine

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Technology Process of N-Benzyl-4-(3,4-dihydro-2,6-naphthyridin-2(1H)-yl)-N-methylcyclohexanamine

There total 4 articles about N-Benzyl-4-(3,4-dihydro-2,6-naphthyridin-2(1H)-yl)-N-methylcyclohexanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-(N-benzyl-N-methylamino)cyclohexanone

: 449175-43-3
1,2,3,4-tetrahydro-2,6-naphthyridine dihydrochloride

: 1365156-20-2
N-Benzyl-4-(3,4-dihydro-2,6-naphthyridin-2(1H)-yl)-N-methylcyclohexanamine

Guidance literature:: 4-(N-benzyl-N-methylamino)cyclohexanone; 1,2,3,4-tetrahydro-2,6-naphthyridine dihydrochloride; In methanol; at 20 ℃; for 5h;

With sodium cyanoborohydride; In methanol; at 0 - 20 ℃; for 16h;

Reference yield:

: 166398-41-0
4-(N-methyl)aminocyclohexane ethylene acetal

: 1365156-20-2
N-Benzyl-4-(3,4-dihydro-2,6-naphthyridin-2(1H)-yl)-N-methylcyclohexanamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / dichloromethane / 0.5 h / 20 °C

1.2: 14 h / 0 - 20 °C

2.1: hydrogenchloride; water / methanol / 16 h / 0 - 20 °C

2.2: pH 8 - 9

3.1: methanol / 5 h / 20 °C

3.2: 16 h / 0 - 20 °C

With hydrogenchloride; water; acetic acid; In methanol; dichloromethane;

Reference yield:

: 4746-97-8
cyclohexanedione monoethylene ketal

: 1365156-20-2
N-Benzyl-4-(3,4-dihydro-2,6-naphthyridin-2(1H)-yl)-N-methylcyclohexanamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid / methanol / 2 h / 20 °C

1.2: 16 h / 0 - 20 °C

2.1: acetic acid / dichloromethane / 0.5 h / 20 °C

2.2: 14 h / 0 - 20 °C

3.1: hydrogenchloride; water / methanol / 16 h / 0 - 20 °C

3.2: pH 8 - 9

4.1: methanol / 5 h / 20 °C

4.2: 16 h / 0 - 20 °C

With hydrogenchloride; water; acetic acid; In methanol; dichloromethane;