6-Brom-2-(4-chlorbenzyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indol-1-on

Base Information

Chemical Name:6-Brom-2-(4-chlorbenzyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indol-1-on
CAS No.:162272-84-6
Molecular Formula:C₁₈H₁₄BrClN₂O
Molecular Weight:389.679
Hs Code.:

Synonyms:6-Brom-2-(4-chlorbenzyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indol-1-on

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Chemical Property of 6-Brom-2-(4-chlorbenzyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indol-1-on

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Technology Process of 6-Brom-2-(4-chlorbenzyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indol-1-on

There total 1 articles about 6-Brom-2-(4-chlorbenzyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indol-1-on which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 104-86-9
4-chlorobenzylamine

: 110977-90-7
6-Brom-4,9-dihydropyrano<3,4-b>indol-1(3H)-on

: 162272-84-6
6-Brom-2-(4-chlorbenzyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indol-1-on

Guidance literature:: at 200 - 240 ℃; for 12h;
DOI:10.1002/ardp.19943271107

Reference yield: 80.0%

: 162272-84-6
6-Brom-2-(4-chlorbenzyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indol-1-on

: 162272-90-4
6-Brom-2-(4-chlorbenzyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; 1.) r.t., 1 h, 2.) reflux, 3 h;
DOI:10.1002/ardp.19943271107

Reference yield:

: 162272-84-6
6-Brom-2-(4-chlorbenzyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indol-1-on

: 244-63-3
betacarboline

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / LiAlH₄ / diethyl ether / 1.) r.t., 1 h, 2.) reflux, 3 h

2: 59 percent / 10percent Pd/C / various solvent(s) / 0.25 h / Heating

With lithium aluminium tetrahydride; palladium on activated charcoal; In diethyl ether;
DOI:10.1002/ardp.19943271107