benzyl dibut-3-enylcarbamate

Base Information

• Chemical Name: benzyl dibut-3-enylcarbamate
• CAS No.: 1226779-54-9
• Molecular Formula: C₁₆H₂₁NO₂
• Molecular Weight: 259.348

Synonyms:benzyl dibut-3-enylcarbamate

Chemical Property of benzyl dibut-3-enylcarbamate

Chemical Property:

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Technology Process of benzyl dibut-3-enylcarbamate

There total 3 articles about benzyl dibut-3-enylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

N-benzyl-N-(but-3-enyl)-but-3-en-1-amine (132365-02-7) + benzyl chloroformate (501-53-1,94274-21-2) → benzyl dibut-3-enylcarbamate (1226779-54-9)

Guidance literature:

In toluene; at 0 - 70 ℃; for 3h; Inert atmosphere;

DOI:10.1016/j.tetlet.2010.12.066

Reference yield:

N-benzyl-N-(but-3-enyl)-but-3-en-1-amine (132365-02-7) + phenyl chloroformate (1885-14-9) → benzyl dibut-3-enylcarbamate (1226779-54-9)

Guidance literature:

In toluene; at 0 - 70 ℃; for 3h;

Reference yield:

benzyl chloroformate (501-53-1,94274-21-2) + phenyl chloroformate (1885-14-9) → benzyl dibut-3-enylcarbamate (1226779-54-9)

Guidance literature:

In toluene; at 0 - 70 ℃; for 3h;

upstream raw materials:

N-benzyl-N-(but-3-enyl)-but-3-en-1-amine

benzyl chloroformate

phenyl chloroformate

Downstream raw materials:

benzyl (R)-3-(tert-butyldimethylsilyloxymethyl)-4-oxopiperidine-1-carboxylate

benzyl bis(3,4-dihydroxybutyl)carbamate

benzyl (R,E)-3-((tert-butyldimethylsilyloxy)methyl)-4-(2-ethoxy-2-oxoethylidene)piperidine-1-carboxylate

benzyl (3R,4R)-4-hydroxy-3-(hydroxymethyl)piperidine-1-carboxylate

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