N-{2-[4,5-dimethoxy-2-(2-oxo-2-phenylethyl)phenyl]-1-methylethyl}formamide

Base Information

Chemical Name:N-{2-[4,5-dimethoxy-2-(2-oxo-2-phenylethyl)phenyl]-1-methylethyl}formamide
CAS No.:894419-50-2
Molecular Formula:C₂₀H₂₃NO₄
Molecular Weight:341.407
Hs Code.:

Synonyms:N-{2-[4,5-dimethoxy-2-(2-oxo-2-phenylethyl)phenyl]-1-methylethyl}formamide

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Chemical Property of N-{2-[4,5-dimethoxy-2-(2-oxo-2-phenylethyl)phenyl]-1-methylethyl}formamide

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Technology Process of N-{2-[4,5-dimethoxy-2-(2-oxo-2-phenylethyl)phenyl]-1-methylethyl}formamide

There total 1 articles about N-{2-[4,5-dimethoxy-2-(2-oxo-2-phenylethyl)phenyl]-1-methylethyl}formamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 93-97-0
benzoic acid anhydride

: 52987-31-2
N-[2-(3,4-dimethoxyphenyl)-1-methyl-ethyl]formamide

: 894419-50-2
N-{2-[4,5-dimethoxy-2-(2-oxo-2-phenylethyl)phenyl]-1-methylethyl}formamide

: 52999-84-5
1-benzyl-6,7-dimethoxy-3-methyl-3,4-dihydro-isoquinoline

Guidance literature:: With PPA; In dichloromethane; at 50 ℃; for 2h;
DOI:10.3987/COM-05-10645

Reference yield: 70.0%

: 894419-50-2
N-{2-[4,5-dimethoxy-2-(2-oxo-2-phenylethyl)phenyl]-1-methylethyl}formamide

: 1-benzylidene-6,7-dimethoxy-3-methyl-3,4-dihydro-1H-isoquinoline-2-carbaldehyde

Guidance literature:: With toluene-4-sulfonic acid; In 1,2-dichloro-ethane; for 0.5h; Heating;
DOI:10.3987/COM-05-10645

Reference yield:

: 894419-50-2
N-{2-[4,5-dimethoxy-2-(2-oxo-2-phenylethyl)phenyl]-1-methylethyl}formamide

: 52999-84-5
1-benzyl-6,7-dimethoxy-3-methyl-3,4-dihydro-isoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / pTsOH / 1,2-dichloro-ethane / 0.5 h / Heating

2: polyphophoric acid / 80 - 100 °C

With polyphophoric acid; toluene-4-sulfonic acid; In 1,2-dichloro-ethane;
DOI:10.3987/COM-05-10645