C₂₆H₁₆F₂N₆O₃S

Base Information

Chemical Name:C₂₆H₁₆F₂N₆O₃S
CAS No.:1415798-19-4
Molecular Formula:C₂₆H₁₆F₂N₆O₃S
Molecular Weight:530.514
Hs Code.:

C<sub>26</sub>H<sub>16</sub>F<sub>2</sub>N<sub>6</sub>O<sub>3</sub>S

Synonyms:C₂₆H₁₆F₂N₆O₃S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₆H₁₆F₂N₆O₃S

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Technology Process of C₂₆H₁₆F₂N₆O₃S

There total 9 articles about C₂₆H₁₆F₂N₆O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1415797-78-2
C₃₄H₂₄F₂N₆O₄S

: 1415798-19-4
C₂₆H₁₆F₂N₆O₃S

Guidance literature:: With trifluoroacetic acid; at 65 ℃; for 3h;

Reference yield:

: 1415797-71-5
4-(4-fluorophenyl)-6-(methoxycarbonyl)-5-oxo-4,5-dihydrothiazolo[5,4-b]pyridine-7-oxy sodium salt

: 1415798-19-4
C₂₆H₁₆F₂N₆O₃S

Guidance literature:: Multi-step reaction with 5 steps

1.1: N,N-dimethyl-formamide / 20 °C / Inert atmosphere

2.1: bis-triphenylphosphine-palladium(II) chloride; triethylsilane; triethylamine / 3 h / 80 °C

3.1: lithium hydroxide monohydrate / tetrahydrofuran; water / 0.5 h / 20 °C

4.1: N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 0.25 h

4.2: 20 °C

5.1: trifluoroacetic acid / 3 h / 65 °C

With triethylsilane; bis-triphenylphosphine-palladium(II) chloride; lithium hydroxide monohydrate; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; water; N,N-dimethyl-formamide;

Reference yield:

: 1415797-72-6
ethyl 5-(N-(4-fluorophenyl)-2-methoxycarbonylacetamido)thiazole-4-formate

: 1415798-19-4
C₂₆H₁₆F₂N₆O₃S

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium methylate / methanol / 20 °C

2.1: N,N-dimethyl-formamide / 20 °C / Inert atmosphere

3.1: bis-triphenylphosphine-palladium(II) chloride; triethylsilane; triethylamine / 3 h / 80 °C

4.1: lithium hydroxide monohydrate / tetrahydrofuran; water / 0.5 h / 20 °C

5.1: N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 0.25 h

5.2: 20 °C

6.1: trifluoroacetic acid / 3 h / 65 °C

With triethylsilane; bis-triphenylphosphine-palladium(II) chloride; lithium hydroxide monohydrate; sodium methylate; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;