4-(4-fluorophenyl)-6-(methoxycarbonyl)-5-oxo-4,5-dihydrothiazolo[5,4-b]pyridine-7-oxy sodium salt

Base Information

Chemical Name:4-(4-fluorophenyl)-6-(methoxycarbonyl)-5-oxo-4,5-dihydrothiazolo[5,4-b]pyridine-7-oxy sodium salt
CAS No.:1415797-71-5
Molecular Formula:C₁₄H₈FN₂O₄S*Na
Molecular Weight:342.283
Hs Code.:

Synonyms:4-(4-fluorophenyl)-6-(methoxycarbonyl)-5-oxo-4,5-dihydrothiazolo[5,4-b]pyridine-7-oxy sodium salt

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Chemical Property of 4-(4-fluorophenyl)-6-(methoxycarbonyl)-5-oxo-4,5-dihydrothiazolo[5,4-b]pyridine-7-oxy sodium salt

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Technology Process of 4-(4-fluorophenyl)-6-(methoxycarbonyl)-5-oxo-4,5-dihydrothiazolo[5,4-b]pyridine-7-oxy sodium salt

There total 3 articles about 4-(4-fluorophenyl)-6-(methoxycarbonyl)-5-oxo-4,5-dihydrothiazolo[5,4-b]pyridine-7-oxy sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1415797-72-6
ethyl 5-(N-(4-fluorophenyl)-2-methoxycarbonylacetamido)thiazole-4-formate

: 1415797-71-5
4-(4-fluorophenyl)-6-(methoxycarbonyl)-5-oxo-4,5-dihydrothiazolo[5,4-b]pyridine-7-oxy sodium salt

Guidance literature:: With sodium methylate; In methanol; at 20 ℃;

Reference yield:

: 371-40-4
4-fluoroaniline

: 1415797-71-5
4-(4-fluorophenyl)-6-(methoxycarbonyl)-5-oxo-4,5-dihydrothiazolo[5,4-b]pyridine-7-oxy sodium salt

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2: potassium tert-butylate / tetrahydrofuran / 2 h / 20 °C

3: 1,2-dichloro-ethane / 2 h / Reflux

4: sodium methylate / methanol / 20 °C

With potassium tert-butylate; sodium methylate; triethylamine; In tetrahydrofuran; methanol; 1,2-dichloro-ethane;

Reference yield:

: 1544-68-9
4-fluorophenyl isothiocyanate

: 1415797-71-5
4-(4-fluorophenyl)-6-(methoxycarbonyl)-5-oxo-4,5-dihydrothiazolo[5,4-b]pyridine-7-oxy sodium salt

Guidance literature:: Multi-step reaction with 3 steps

1: potassium tert-butylate / tetrahydrofuran / 2 h / 20 °C

2: 1,2-dichloro-ethane / 2 h / Reflux

3: sodium methylate / methanol / 20 °C

With potassium tert-butylate; sodium methylate; In tetrahydrofuran; methanol; 1,2-dichloro-ethane;