bromure d'o-(N-phenylacetylamino)benzyltriphenylphosphonium

Base Information

• Chemical Name: bromure d'o-(N-phenylacetylamino)benzyltriphenylphosphonium
• CAS No.: 104894-13-5
• Molecular Formula: Br*C₃₃H₂₉NOP
• Molecular Weight: 566.477
• Mol file: 104894-13-5.mol

Synonyms:bromure d'o-(N-phenylacetylamino)benzyltriphenylphosphonium

Chemical Property of bromure d'o-(N-phenylacetylamino)benzyltriphenylphosphonium

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of bromure d'o-(N-phenylacetylamino)benzyltriphenylphosphonium

There total 3 articles about bromure d'o-(N-phenylacetylamino)benzyltriphenylphosphonium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

bromure d'o-(N-phenylamino)benzyltriphenylphosphonium (78133-85-4) + acetyl chloride (75-36-5) → bromure d'o-(N-phenylacetylamino)benzyltriphenylphosphonium (104894-13-5)

Guidance literature:

With pyridine; In dichloromethane; for 5h; Heating;

DOI:10.1016/S0040-4020(01)96783-3

Reference yield:

triphenylphosphine (603-35-0) → bromure d'o-(N-phenylacetylamino)benzyltriphenylphosphonium (104894-13-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 76 percent / HBr / CH₂Cl₂

2: 86 percent / pyridine / CH₂Cl₂ / 5 h / Heating

With pyridine; hydrogen bromide; In dichloromethane;

DOI:10.1016/S0040-4020(01)96783-3

Reference yield:

N-Phenyl-o-(hydroxymethyl)aniline (53044-24-9) → bromure d'o-(N-phenylacetylamino)benzyltriphenylphosphonium (104894-13-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 76 percent / HBr / CH₂Cl₂

2: 86 percent / pyridine / CH₂Cl₂ / 5 h / Heating

With pyridine; hydrogen bromide; In dichloromethane;

DOI:10.1016/S0040-4020(01)96783-3

upstream raw materials:

bromure d'o-(N-phenylamino)benzyltriphenylphosphonium

acetyl chloride

N-Phenyl-o-(hydroxymethyl)aniline

triphenylphosphine

Downstream raw materials:

2-methyl-1-phenyl-1H-indole

Refernces