[4-chloro-2-({[4-chloro-3-(trifluoromethyl)phenyl]sulfonyl}amino)phenyl]methylphosphinic acid

Base Information

Chemical Name:[4-chloro-2-({[4-chloro-3-(trifluoromethyl)phenyl]sulfonyl}amino)phenyl]methylphosphinic acid
CAS No.:1382801-48-0
Molecular Formula:C₁₄H₁₁Cl₂F₃NO₄PS
Molecular Weight:448.187
Hs Code.:

Synonyms:[4-chloro-2-({[4-chloro-3-(trifluoromethyl)phenyl]sulfonyl}amino)phenyl]methylphosphinic acid

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Chemical Property of [4-chloro-2-({[4-chloro-3-(trifluoromethyl)phenyl]sulfonyl}amino)phenyl]methylphosphinic acid

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Technology Process of [4-chloro-2-({[4-chloro-3-(trifluoromethyl)phenyl]sulfonyl}amino)phenyl]methylphosphinic acid

There total 4 articles about [4-chloro-2-({[4-chloro-3-(trifluoromethyl)phenyl]sulfonyl}amino)phenyl]methylphosphinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1382801-44-6
Ethyl [4-chloro-2-({[4-chloro-3-(trifluoromethyl)phenyl]sulfonyl}amino)phenyl]methylphosphinate

: 1382801-48-0
[4-chloro-2-({[4-chloro-3-(trifluoromethyl)phenyl]sulfonyl}amino)phenyl]methylphosphinic acid

Guidance literature:: Ethyl [4-chloro-2-({[4-chloro-3-(trifluoromethyl)phenyl]sulfonyl}amino)phenyl]methylphosphinate; With 1-(Trimethylsilyl)imidazole; In chloroform; at 20 ℃; for 0.5h;

With water; In chloroform;

Reference yield:

: 6828-35-9
5-chloro-2-iodoaniline

: 1382801-48-0
[4-chloro-2-({[4-chloro-3-(trifluoromethyl)phenyl]sulfonyl}amino)phenyl]methylphosphinic acid

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 100 °C

2: caesium carbonate / copper(l) iodide; N,N`-dimethylethylenediamine / toluene / 110 °C / sealed tube

3: 1-(Trimethylsilyl)imidazole / chloroform / 0.5 h / 20 °C

With pyridine; caesium carbonate; 1-(Trimethylsilyl)imidazole; copper(l) iodide; N,N`-dimethylethylenediamine; In chloroform; toluene;

Reference yield:

: 1382801-61-7
4-Chloro-N-(5-chloro-2-iodophenyl)-3-(trifluoromethyl)benzenesulfonamide

: 1382801-48-0
[4-chloro-2-({[4-chloro-3-(trifluoromethyl)phenyl]sulfonyl}amino)phenyl]methylphosphinic acid

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / copper(l) iodide; N,N`-dimethylethylenediamine / toluene / 110 °C / sealed tube

2: 1-(Trimethylsilyl)imidazole / chloroform / 0.5 h / 20 °C

With caesium carbonate; 1-(Trimethylsilyl)imidazole; copper(l) iodide; N,N`-dimethylethylenediamine; In chloroform; toluene;