4-Chloro-N-(5-chloro-2-iodophenyl)-3-(trifluoromethyl)benzenesulfonamide

Base Information

• Chemical Name: 4-Chloro-N-(5-chloro-2-iodophenyl)-3-(trifluoromethyl)benzenesulfonamide
• CAS No.: 1382801-61-7
• Molecular Formula: C₁₃H₇Cl₂F₃INO₂S
• Molecular Weight: 496.076

Synonyms:4-Chloro-N-(5-chloro-2-iodophenyl)-3-(trifluoromethyl)benzenesulfonamide

Chemical Property of 4-Chloro-N-(5-chloro-2-iodophenyl)-3-(trifluoromethyl)benzenesulfonamide

Chemical Property:

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Technology Process of 4-Chloro-N-(5-chloro-2-iodophenyl)-3-(trifluoromethyl)benzenesulfonamide

There total 1 articles about 4-Chloro-N-(5-chloro-2-iodophenyl)-3-(trifluoromethyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

4-chloro-3-trifluoromethylbenzenesulfonyl chloride (32333-53-2) + 5-chloro-2-iodoaniline (6828-35-9) → 4-Chloro-N-(5-chloro-2-iodophenyl)-3-(trifluoromethyl)benzenesulfonamide (1382801-61-7)

Guidance literature:

With pyridine; at 100 ℃;

Reference yield: 57.0%

ethyl methylphosphinate (16391-07-4) + 4-Chloro-N-(5-chloro-2-iodophenyl)-3-(trifluoromethyl)benzenesulfonamide (1382801-61-7) → Ethyl [4-chloro-2-({[4-chloro-3-(trifluoromethyl)phenyl]sulfonyl}amino)phenyl]methylphosphinate (1382801-44-6)

Guidance literature:

With caesium carbonate; copper(l) iodide; N,N`-dimethylethylenediamine; In toluene; at 110 ℃; sealed tube;

Reference yield: 35.0%

4-Chloro-N-(5-chloro-2-iodophenyl)-3-(trifluoromethyl)benzenesulfonamide (1382801-61-7) + ethyl Phenylphosphinate (172487-18-2,2511-09-3) → Ethyl (4-chloro-2-(4-chloro-3-(trifluoromethyl)phenylsulfonamido)phenyl)(phenyl)phosphinate (1382801-56-0)

Guidance literature:

With triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 100 ℃; sealed tube;

upstream raw materials:

4-chloro-3-trifluoromethylbenzenesulfonyl chloride

5-chloro-2-iodoaniline

Downstream raw materials:

Ethyl [4-chloro-2-({[4-chloro-3-(trifluoromethyl)phenyl]sulfonyl}amino)phenyl]methylphosphinate

4-Chloro-N-{5-chloro-2-[methyl(morpholin-4-yl)phosphoryl]phenyl}-3-(trifluoromethyl)benzenesulfonamide

[4-chloro-2-({[4-chloro-3-(trifluoromethyl)phenyl]sulfonyl}amino)phenyl]methylphosphinic acid

Ethyl (4-chloro-2-(4-chloro-3-(trifluoromethyl)phenylsulfonamido)phenyl)(phenyl)phosphinate

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