6-(3-(N-t-butoxycarbonyl-N-methylamino)-4-nitrophenoxymethyl)-4-methyl-2-propyl-1-[2'-(1-triphenylmethyl-1H-tetrazol-5-yl)biphenyl-4-ylmethyl]-1H-benzimidazole

Base Information

Chemical Name:6-(3-(N-t-butoxycarbonyl-N-methylamino)-4-nitrophenoxymethyl)-4-methyl-2-propyl-1-[2'-(1-triphenylmethyl-1H-tetrazol-5-yl)biphenyl-4-ylmethyl]-1H-benzimidazole
CAS No.:1350439-63-2
Molecular Formula:C₅₇H₅₄N₈O₅
Molecular Weight:931.106
Hs Code.:

6-(3-(N-t-butoxycarbonyl-N-methylamino)-4-nitrophenoxymethyl)-4-methyl-2-propyl-1-[2'-(1-triphenylmethyl-1H-tetrazol-5-yl)biphenyl-4-ylmethyl]-1H-benzimidazole

Synonyms:6-(3-(N-t-butoxycarbonyl-N-methylamino)-4-nitrophenoxymethyl)-4-methyl-2-propyl-1-[2'-(1-triphenylmethyl-1H-tetrazol-5-yl)biphenyl-4-ylmethyl]-1H-benzimidazole

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Chemical Property of 6-(3-(N-t-butoxycarbonyl-N-methylamino)-4-nitrophenoxymethyl)-4-methyl-2-propyl-1-[2'-(1-triphenylmethyl-1H-tetrazol-5-yl)biphenyl-4-ylmethyl]-1H-benzimidazole

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Technology Process of 6-(3-(N-t-butoxycarbonyl-N-methylamino)-4-nitrophenoxymethyl)-4-methyl-2-propyl-1-[2'-(1-triphenylmethyl-1H-tetrazol-5-yl)biphenyl-4-ylmethyl]-1H-benzimidazole

There total 2 articles about 6-(3-(N-t-butoxycarbonyl-N-methylamino)-4-nitrophenoxymethyl)-4-methyl-2-propyl-1-[2'-(1-triphenylmethyl-1H-tetrazol-5-yl)biphenyl-4-ylmethyl]-1H-benzimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 299176-17-3
N-(2-nitro-5-chlorophenyl)-N-methylcarbamic acid t-butyl ester

: 1046423-49-7
6-hydroxymethyl-4-methyl-2-propyl-1-[2'-(1-triphenylmethyl-1H-tetrazol-5-yl)biphenyl-4-ylmethyl]-1H-benzimidazole

: 1350439-63-2
6-(3-(N-t-butoxycarbonyl-N-methylamino)-4-nitrophenoxymethyl)-4-methyl-2-propyl-1-[2'-(1-triphenylmethyl-1H-tetrazol-5-yl)biphenyl-4-ylmethyl]-1H-benzimidazole

Guidance literature:: 6-hydroxymethyl-4-methyl-2-propyl-1-[2'-(1-triphenylmethyl-1H-tetrazol-5-yl)biphenyl-4-ylmethyl]-1H-benzimidazole; With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 1.71667h; Cooling with ice;

N-(2-nitro-5-chlorophenyl)-N-methylcarbamic acid t-butyl ester; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil; at 20 ℃;

Reference yield:

: 1046423-45-3
4-methyl-2-propyl-1-[2'-(1-triphenylmethyl-1H-tetrazol-5-yl)biphenyl-4-ylmethyl]-1H-benzimidazole-6-carboxylic acid methyl ester

: 1350439-63-2
6-(3-(N-t-butoxycarbonyl-N-methylamino)-4-nitrophenoxymethyl)-4-methyl-2-propyl-1-[2'-(1-triphenylmethyl-1H-tetrazol-5-yl)biphenyl-4-ylmethyl]-1H-benzimidazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 20 °C

2.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide; mineral oil / 1.72 h / 20 °C / Cooling with ice

2.2: 20 °C

With lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;