Technology Process of C29H26N2O4S
There total 9 articles about C29H26N2O4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate;
In
1,2-dimethoxyethane; water;
at 80 ℃;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium hydroxide / ethylene glycol / 6 h / 160 °C
1.2: pH 3 - 4
2.1: sulfuric acid / 4 h / 65 °C
3.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 90 °C / Inert atmosphere
4.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane / 80 °C / Inert atmosphere
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sulfuric acid; sodium carbonate; potassium hydroxide;
In
1,4-dioxane; 1,2-dimethoxyethane; water; ethylene glycol;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: tetrabutylammomium bromide; potassium hydroxide / water; toluene / 65 °C
2.1: potassium hydroxide / ethylene glycol / 6 h / 160 °C
2.2: pH 3 - 4
3.1: sulfuric acid / 4 h / 65 °C
4.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 90 °C / Inert atmosphere
5.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane / 80 °C / Inert atmosphere
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sulfuric acid; tetrabutylammomium bromide; sodium carbonate; potassium hydroxide;
In
1,4-dioxane; 1,2-dimethoxyethane; water; ethylene glycol; toluene;