(+/-)-syn-2-[2-(4-chlorophenylselanyl)ethyl]-3-methyl-pent-4-ynoic acid amide

Base Information

Chemical Name:(+/-)-syn-2-[2-(4-chlorophenylselanyl)ethyl]-3-methyl-pent-4-ynoic acid amide
CAS No.:145215-55-0
Molecular Formula:C₁₄H₁₆ClNOSe
Molecular Weight:328.7
Hs Code.:

Synonyms:(+/-)-syn-2-[2-(4-chlorophenylselanyl)ethyl]-3-methyl-pent-4-ynoic acid amide

Suppliers and Price of (+/-)-syn-2-[2-(4-chlorophenylselanyl)ethyl]-3-methyl-pent-4-ynoic acid amide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (+/-)-syn-2-[2-(4-chlorophenylselanyl)ethyl]-3-methyl-pent-4-ynoic acid amide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (+/-)-syn-2-[2-(4-chlorophenylselanyl)ethyl]-3-methyl-pent-4-ynoic acid amide

There total 6 articles about (+/-)-syn-2-[2-(4-chlorophenylselanyl)ethyl]-3-methyl-pent-4-ynoic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 145215-54-9
(+/-)-syn-2-[2-(4-chlorophenylselanyl)ethyl]-3-methyl-pent-4-ynoic acid

: 145215-55-0
(+/-)-syn-2-[2-(4-chlorophenylselanyl)ethyl]-3-methyl-pent-4-ynoic acid amide

Guidance literature:: With ammonia; isobutyl chloroformate; -78 deg C to room temperature;
DOI:10.1016/S0040-4039(00)60942-5

Reference yield:

: C₁₄H₁₅ClO₂SeC₅H₈O₂

: 145215-55-0
(+/-)-syn-2-[2-(4-chlorophenylselanyl)ethyl]-3-methyl-pent-4-ynoic acid amide

Guidance literature:: With ammonia; In tetrahydrofuran; at -78 - 20 ℃;
DOI:10.1021/jo005531k

Reference yield:

: 20541-49-5
bis(p-chlorophenyl) diselenide

: 145215-55-0
(+/-)-syn-2-[2-(4-chlorophenylselanyl)ethyl]-3-methyl-pent-4-ynoic acid amide

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH / tetrahydrofuran / 1.5 h / Heating

1.2: 72 percent / tetrahydrofuran; hexamethylphosphoric acid triamide / 3 h / Heating

2.1: Et₃N / tetrahydrofuran / 0.67 h / 0 °C

3.1: 0.11 g / NH₃ / tetrahydrofuran / -78 - 20 °C

With ammonia; sodium hydride; triethylamine; In tetrahydrofuran;
DOI:10.1021/jo005531k