(S)-2-(4-aminomethyl-benzylamino)-3-phenyl-propionic acid cyclopentyl ester

Base Information

Chemical Name:(S)-2-(4-aminomethyl-benzylamino)-3-phenyl-propionic acid cyclopentyl ester
CAS No.:914606-09-0
Molecular Formula:C₂₂H₂₈N₂O₂
Molecular Weight:352.477
Hs Code.:

Synonyms:(S)-2-(4-aminomethyl-benzylamino)-3-phenyl-propionic acid cyclopentyl ester

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Chemical Property of (S)-2-(4-aminomethyl-benzylamino)-3-phenyl-propionic acid cyclopentyl ester

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Technology Process of (S)-2-(4-aminomethyl-benzylamino)-3-phenyl-propionic acid cyclopentyl ester

There total 5 articles about (S)-2-(4-aminomethyl-benzylamino)-3-phenyl-propionic acid cyclopentyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 914606-08-9
(S)-2-[4-(tert-butoxycarbonylamino-methyl)-benzylamino]-3-phenyl-propionic acid cyclopentyl ester

: 914606-09-0
(S)-2-(4-aminomethyl-benzylamino)-3-phenyl-propionic acid cyclopentyl ester

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 1h;

Reference yield:

: 39895-56-2
4-hydroxymethyl-benzylamine

: 914606-09-0
(S)-2-(4-aminomethyl-benzylamino)-3-phenyl-propionic acid cyclopentyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydrogencarbonate / tetrahydrofuran; water / 0 °C / pH > 9

2.1: lithium aluminium tetrahydride / tetrahydrofuran; 1,4-dioxane / 16.25 h / 0 - 20 °C

3.1: Dess-Martin periodane / dichloromethane / 3 h / -78 - 20 °C

4.1: 1,1-dichloroethane / 0.25 h / 20 °C

4.2: 1 h

5.1: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C

With hydrogenchloride; lithium aluminium tetrahydride; sodium hydrogencarbonate; Dess-Martin periodane; In tetrahydrofuran; 1,4-dioxane; 1,1-dichloroethane; dichloromethane; water;

Reference yield:

: 33233-67-9
4-(tert-Butoxycarbonylaminomethyl)benzoic acid

: 914606-09-0
(S)-2-(4-aminomethyl-benzylamino)-3-phenyl-propionic acid cyclopentyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran; 1,4-dioxane / 16.25 h / 0 - 20 °C

2.1: Dess-Martin periodane / dichloromethane / 3 h / -78 - 20 °C

3.1: 1,1-dichloroethane / 0.25 h / 20 °C

3.2: 1 h

4.1: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C

With hydrogenchloride; lithium aluminium tetrahydride; Dess-Martin periodane; In tetrahydrofuran; 1,4-dioxane; 1,1-dichloroethane; dichloromethane;