(S)-2-[4-(tert-butoxycarbonylamino-methyl)-benzylamino]-3-phenyl-propionic acid cyclopentyl ester

Base Information

Chemical Name:(S)-2-[4-(tert-butoxycarbonylamino-methyl)-benzylamino]-3-phenyl-propionic acid cyclopentyl ester
CAS No.:914606-08-9
Molecular Formula:C₂₇H₃₆N₂O₄
Molecular Weight:452.594
Hs Code.:

Synonyms:(S)-2-[4-(tert-butoxycarbonylamino-methyl)-benzylamino]-3-phenyl-propionic acid cyclopentyl ester

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Chemical Property of (S)-2-[4-(tert-butoxycarbonylamino-methyl)-benzylamino]-3-phenyl-propionic acid cyclopentyl ester

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Technology Process of (S)-2-[4-(tert-butoxycarbonylamino-methyl)-benzylamino]-3-phenyl-propionic acid cyclopentyl ester

There total 4 articles about (S)-2-[4-(tert-butoxycarbonylamino-methyl)-benzylamino]-3-phenyl-propionic acid cyclopentyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 39895-56-2
4-hydroxymethyl-benzylamine

: 914606-08-9
(S)-2-[4-(tert-butoxycarbonylamino-methyl)-benzylamino]-3-phenyl-propionic acid cyclopentyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydrogencarbonate / tetrahydrofuran; water / 0 °C / pH > 9

2.1: lithium aluminium tetrahydride / tetrahydrofuran; 1,4-dioxane / 16.25 h / 0 - 20 °C

3.1: Dess-Martin periodane / dichloromethane / 3 h / -78 - 20 °C

4.1: 1,1-dichloroethane / 0.25 h / 20 °C

4.2: 1 h

With lithium aluminium tetrahydride; sodium hydrogencarbonate; Dess-Martin periodane; In tetrahydrofuran; 1,4-dioxane; 1,1-dichloroethane; dichloromethane; water;

Reference yield:

: 205180-02-5
(S)-2-amino-3-phenyl-propionic acid cyclopentyl ester

: 156866-52-3
tert-butyl N-(4-formylbenzyl)carbamate

: 914606-08-9
(S)-2-[4-(tert-butoxycarbonylamino-methyl)-benzylamino]-3-phenyl-propionic acid cyclopentyl ester

Guidance literature:: (S)-2-amino-3-phenyl-propionic acid cyclopentyl ester; tert-butyl N-(4-formylbenzyl)carbamate; In 1,1-dichloroethane; at 20 ℃; for 0.25h;

With sodium tris(acetoxy)borohydride; acetic acid; In 1,1-dichloroethane; for 1h;

Reference yield:

: 33233-67-9
4-(tert-Butoxycarbonylaminomethyl)benzoic acid

: 914606-08-9
(S)-2-[4-(tert-butoxycarbonylamino-methyl)-benzylamino]-3-phenyl-propionic acid cyclopentyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran; 1,4-dioxane / 16.25 h / 0 - 20 °C

2.1: Dess-Martin periodane / dichloromethane / 3 h / -78 - 20 °C

3.1: 1,1-dichloroethane / 0.25 h / 20 °C

3.2: 1 h

With lithium aluminium tetrahydride; Dess-Martin periodane; In tetrahydrofuran; 1,4-dioxane; 1,1-dichloroethane; dichloromethane;