[4-[6-(allylmethylamino)hexyloxy]-2-methoxyphenyl](4-bromophenyl)methanone

Base Information

• Chemical Name: [4-[6-(allylmethylamino)hexyloxy]-2-methoxyphenyl](4-bromophenyl)methanone
• CAS No.: 192437-67-5
• Molecular Formula: C₂₄H₃₀BrNO₃
• Molecular Weight: 460.411

Synonyms:[4-[6-(allylmethylamino)hexyloxy]-2-methoxyphenyl](4-bromophenyl)methanone

Chemical Property of [4-[6-(allylmethylamino)hexyloxy]-2-methoxyphenyl](4-bromophenyl)methanone

Chemical Property:

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Technology Process of [4-[6-(allylmethylamino)hexyloxy]-2-methoxyphenyl](4-bromophenyl)methanone

There total 1 articles about [4-[6-(allylmethylamino)hexyloxy]-2-methoxyphenyl](4-bromophenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sodium methylate (124-41-4) + [4-[6-(allyl-methyl-amino)-hexyloxy]-2-fluoro-phenyl]-(4-bromo-phenyl)-methanone (161582-11-2) → [4-[6-(allylmethylamino)hexyloxy]-2-methoxyphenyl](4-bromophenyl)methanone (192437-67-5)

Guidance literature:

In tetrahydrofuran; methanol; for 1h; Heating;

DOI:10.1021/jm021120f

Reference yield: 100.0%

[4-[6-(allylmethylamino)hexyloxy]-2-methoxyphenyl](4-bromophenyl)methanone (192437-67-5) → [4-[6-(allylmethylamino)hexyloxy]-2-hydroxyphenyl](4-bromophenyl)methanone (192435-54-4)

Guidance literature:

With hydrogen bromide; acetic acid; at 90 ℃; for 2h;

DOI:10.1021/jm021120f

Reference yield:

[4-[6-(allyl-methyl-amino)-hexyloxy]-2-methoxy-phenyl]-(4-bromo-phenyl)-methanone.fumarate (192437-68-6) + (2E)-but-2-enedioic acid (110-17-8,26099-09-2) + [4-[6-(allyl-methyl-amino)-hexyloxy]-2-fluoro-phenyl]-(4-bromo-phenyl)-methanone (161582-11-2) + [4-[6-(allylmethylamino)hexyloxy]-2-methoxyphenyl](4-bromophenyl)methanone (192437-67-5) → [4-[6-(allyl-methyl-amino)-hexyloxy]-2-hydroxy-phenyl]-(4-bromo-phenyl)-methanone.fumarate (192435-55-5)

Guidance literature:

With hydrogen bromide; sodium methylate; In tetrahydrofuran; methanol; ethanol; dichloromethane; acetic acid;

upstream raw materials:

sodium methylate

[4-[6-(allyl-methyl-amino)-hexyloxy]-2-fluoro-phenyl]-(4-bromo-phenyl)-methanone

Downstream raw materials:

[4-[6-(allylmethylamino)hexyloxy]-2-hydroxyphenyl](4-bromophenyl)methanone

(RS)-5-[6-(allyl-methyl-amino)-hexyloxy]-2-(1-(4-bromo-phenyl)-1-hydroxy-allyl]-phenol

[4-[6-(allyl-methyl-amino)-hexyloxy]-2-hydroxy-phenyl]-(4-bromo-phenyl)-methanone.fumarate

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