2,10-dibenzyloxy-12,13-dihydro-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-6-methyl-5,7-(6H)-dione

Base Information

• Chemical Name: 2,10-dibenzyloxy-12,13-dihydro-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-6-methyl-5,7-(6H)-dione
• CAS No.: 174402-52-9
• Molecular Formula: C₃₅H₂₅N₃O₄
• Molecular Weight: 551.601

Synonyms:2,10-dibenzyloxy-12,13-dihydro-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-6-methyl-5,7-(6H)-dione

Chemical Property of 2,10-dibenzyloxy-12,13-dihydro-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-6-methyl-5,7-(6H)-dione

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Technology Process of 2,10-dibenzyloxy-12,13-dihydro-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-6-methyl-5,7-(6H)-dione

There total 1 articles about 2,10-dibenzyloxy-12,13-dihydro-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-6-methyl-5,7-(6H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

2,5-dihydro-3,4-bis-(6-benzyloxy-1H-indol-3-yl)-1-methyl-1H-pyrrole-2,5-dione (174402-51-8) → 2,10-dibenzyloxy-12,13-dihydro-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-6-methyl-5,7-(6H)-dione (174402-52-9)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In toluene; for 0.666667h; Heating;

DOI:10.1016/0040-4020(96)00372-9

Reference yield: 99.0%

2,3,4,6-tetra-O-benzyl-D-galactopyranosyl chloride (4291-68-3) + 2,10-dibenzyloxy-12,13-dihydro-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-6-methyl-5,7-(6H)-dione (174402-52-9) → C69H59N3O9 (270918-02-0)

Guidance literature:

With potassium hydroxide; sodium sulfate; In acetonitrile;

DOI:10.1016/S0960-894X(00)00004-4

Reference yield: 99.0%

2,3,4-tri-O-benzyl-6-deoxy-α,β-D-glucopyranosyl chloride (270917-97-0) + 2,10-dibenzyloxy-12,13-dihydro-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-6-methyl-5,7-(6H)-dione (174402-52-9) → C62H53N3O8 (270918-05-3)

Guidance literature:

With potassium hydroxide; sodium sulfate; In acetonitrile;

DOI:10.1016/S0960-894X(00)00004-4

upstream raw materials:

2,5-dihydro-3,4-bis-(6-benzyloxy-1H-indol-3-yl)-1-methyl-1H-pyrrole-2,5-dione

Downstream raw materials:

12,13-dihydro-2,10-dibenzyloxy-13-(β-D-2,3,4,6-tetra-O-benzylglucopyranosyl)-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-6-methyl-5,7(6H)-dione

C₆₉H₅₉N₃O₉

C₆₁H₅₁N₃O₈

C₆₂H₅₃N₃O₈

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