12,13-dihydro-2,10-dibenzyloxy-13-(β-D-2,3,4,6-tetra-O-benzylglucopyranosyl)-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-6-methyl-5,7(6H)-dione

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Chemical Name:12,13-dihydro-2,10-dibenzyloxy-13-(β-D-2,3,4,6-tetra-O-benzylglucopyranosyl)-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-6-methyl-5,7(6H)-dione
CAS No.:174402-48-3
Molecular Formula:C₆₉H₅₉N₃O₉
Molecular Weight:1074.24
Hs Code.:

Synonyms:12,13-dihydro-2,10-dibenzyloxy-13-(β-D-2,3,4,6-tetra-O-benzylglucopyranosyl)-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-6-methyl-5,7(6H)-dione

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Chemical Property of 12,13-dihydro-2,10-dibenzyloxy-13-(β-D-2,3,4,6-tetra-O-benzylglucopyranosyl)-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-6-methyl-5,7(6H)-dione

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Technology Process of 12,13-dihydro-2,10-dibenzyloxy-13-(β-D-2,3,4,6-tetra-O-benzylglucopyranosyl)-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-6-methyl-5,7(6H)-dione

There total 5 articles about 12,13-dihydro-2,10-dibenzyloxy-13-(β-D-2,3,4,6-tetra-O-benzylglucopyranosyl)-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-6-methyl-5,7(6H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: C₇₅H₇₃N₃O₁₀Si

: 174402-48-3
12,13-dihydro-2,10-dibenzyloxy-13-(β-D-2,3,4,6-tetra-O-benzylglucopyranosyl)-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-6-methyl-5,7(6H)-dione

Guidance literature:: With molecular sieve; tetrabutyl ammonium fluoride; In tetrahydrofuran; at 50 ℃; for 2h;

Reference yield: 84.0%

: 174402-47-2
3-(6-Benzyloxy-1H-indol-3-yl)-4-[6-benzyloxy-1-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-1H-indol-3-yl]-1-methyl-pyrrole-2,5-dione

: 174402-48-3
12,13-dihydro-2,10-dibenzyloxy-13-(β-D-2,3,4,6-tetra-O-benzylglucopyranosyl)-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-6-methyl-5,7(6H)-dione

Guidance literature:: With copper dichloride; In butanone; at 25 ℃; for 2h;
DOI:10.1016/S0040-4020(97)00286-X

Reference yield: 83.0%

: 4291-68-3,25320-59-6,41110-63-8,67068-83-1,67773-44-8,69237-96-3,92470-93-4,93601-69-5,113829-62-2
1-chloro-2,3,4,6-tetra-O-benzyl-D-glucopyranoside

: 174402-52-9
2,10-dibenzyloxy-12,13-dihydro-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-6-methyl-5,7-(6H)-dione

: 174402-48-3
12,13-dihydro-2,10-dibenzyloxy-13-(β-D-2,3,4,6-tetra-O-benzylglucopyranosyl)-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-6-methyl-5,7(6H)-dione

Guidance literature:: 1-chloro-2,3,4,6-tetra-O-benzyl-D-glucopyranoside; 2,10-dibenzyloxy-12,13-dihydro-5H-indolo[2,3-a]pyrrolo[3,4-c]carbazole-6-methyl-5,7-(6H)-dione; In tert-butyl methyl ether; at 20 ℃; for 0.5h;

With potassium hydroxide; In tert-butyl methyl ether; water; at 20 ℃; for 0.166667 - 0.583333h;

Aliquat 336; In tert-butyl methyl ether; water; at 20 - 25 ℃; for 3 - 4.00417h; Product distribution / selectivity;