Technology Process of 2-methyl-7-phenyl-1H-indole
There total 5 articles about 2-methyl-7-phenyl-1H-indole which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dimethyl sulfate / 2 h / 70 °C / Inert atmosphere
2: diphenyl hydrogen phosphate; Rh2(esp)2 / dichloromethane / 0.17 h / 0 °C / Inert atmosphere
With
diphenyl hydrogen phosphate; Rh2(esp)2; dimethyl sulfate;
In
dichloromethane;
DOI:10.1021/acs.orglett.5b03064
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane
2: dimethyl sulfate / 2 h / 70 °C / Inert atmosphere
3: diphenyl hydrogen phosphate; Rh2(esp)2 / dichloromethane / 0.17 h / 0 °C / Inert atmosphere
With
diphenyl hydrogen phosphate; Rh2(esp)2; 3-chloro-benzenecarboperoxoic acid; dimethyl sulfate;
In
dichloromethane;
DOI:10.1021/acs.orglett.5b03064
- Guidance literature:
-
Multi-step reaction with 4 steps
1: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / 1,2-dimethoxyethane; water / 12 h / 80 °C / Inert atmosphere
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane
3: dimethyl sulfate / 2 h / 70 °C / Inert atmosphere
4: diphenyl hydrogen phosphate; Rh2(esp)2 / dichloromethane / 0.17 h / 0 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; diphenyl hydrogen phosphate; Rh2(esp)2; sodium carbonate; 3-chloro-benzenecarboperoxoic acid; dimethyl sulfate;
In
1,2-dimethoxyethane; dichloromethane; water;
DOI:10.1021/acs.orglett.5b03064
