C₂₄H₂₆ClF₂NO₄S

Base Information

Chemical Name:C₂₄H₂₆ClF₂NO₄S
CAS No.:471903-70-5
Molecular Formula:C₂₄H₂₆ClF₂NO₄S
Molecular Weight:497.991
Hs Code.:

C<sub>24</sub>H<sub>26</sub>ClF<sub>2</sub>NO<sub>4</sub>S

Synonyms:C₂₄H₂₆ClF₂NO₄S

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Chemical Property of C₂₄H₂₆ClF₂NO₄S

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Technology Process of C₂₄H₂₆ClF₂NO₄S

There total 9 articles about C₂₄H₂₆ClF₂NO₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 110-91-8,99108-56-2
morpholine

: 471903-69-2
[4-(4-chloro-benzenesulfonyl)-4-(2,5-difluoro-phenyl)-cyclohexyl]-acetic acid

: 471903-70-5
C₂₄H₂₆ClF₂NO₄S

Guidance literature:: morpholine; [4-(4-chloro-benzenesulfonyl)-4-(2,5-difluoro-phenyl)-cyclohexyl]-acetic acid; With benzotriazol-1-ol; triethylamine; In tetrahydrofuran; at 20 ℃; for 0.166667h;

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; for 24h;

Reference yield:

: 470716-52-0
2-[[(4-chlorophenyl)thio]methyl]-1,4-difluorobenzene

: 471903-70-5
C₂₄H₂₆ClF₂NO₄S

Guidance literature:: Multi-step reaction with 7 steps

1: m-chloroperoxybenzoic acid / dichloromethane / 2 h

2: potassium tert-butylate / tetrahydrofuran / 2 h

3: water; sodium chloride / dimethyl sulfoxide / 2 h / 150 °C

4: sodium hydride / tetrahydrofuran / 19.33 h / 20 °C

5: sodium tetrahydroborate / nickel dichloride / ethanol / 0.33 h / 20 °C

6: lithium hydroxide / ethanol / 5 h / 20 °C

7: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / tetrahydrofuran / 24.17 h / 20 °C

With lithium hydroxide; sodium tetrahydroborate; m-chloroperoxybenzoic acid; potassium tert-butylate; water; sodium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium chloride; nickel dichloride; In tetrahydrofuran; ethanol; dichloromethane; dimethyl sulfoxide;

Reference yield:

: 471903-20-5
4-[(4-chlorophenyl)sulfonyl]-4-(2,5-difluorophenyl)cyclohexanone

: 471903-70-5
C₂₄H₂₆ClF₂NO₄S

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydride / tetrahydrofuran / 19.33 h / 20 °C

2: sodium tetrahydroborate / nickel dichloride / ethanol / 0.33 h / 20 °C

3: lithium hydroxide / ethanol / 5 h / 20 °C

4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / tetrahydrofuran / 24.17 h / 20 °C

With lithium hydroxide; sodium tetrahydroborate; sodium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; nickel dichloride; In tetrahydrofuran; ethanol;