2-(4-chloro-3-methylphenyl)-2-oxoethyl (3-{[(benzyloxy)carbonyl]amino}oxetan-3-yl)acetate

Base Information

Chemical Name:2-(4-chloro-3-methylphenyl)-2-oxoethyl (3-{[(benzyloxy)carbonyl]amino}oxetan-3-yl)acetate
CAS No.:1432023-97-6
Molecular Formula:C₂₂H₂₂ClNO₆
Molecular Weight:431.873
Hs Code.:

Synonyms:2-(4-chloro-3-methylphenyl)-2-oxoethyl (3-{[(benzyloxy)carbonyl]amino}oxetan-3-yl)acetate

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Chemical Property of 2-(4-chloro-3-methylphenyl)-2-oxoethyl (3-{[(benzyloxy)carbonyl]amino}oxetan-3-yl)acetate

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Technology Process of 2-(4-chloro-3-methylphenyl)-2-oxoethyl (3-{[(benzyloxy)carbonyl]amino}oxetan-3-yl)acetate

There total 3 articles about 2-(4-chloro-3-methylphenyl)-2-oxoethyl (3-{[(benzyloxy)carbonyl]amino}oxetan-3-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1432024-10-6
2-(3-(((benzyloxy)carbonyl)amino)oxetan-3-yl)acetic acid

: 205178-80-9
2-Bromo-1-(4-chloro-3-methylphenyl)ethan-1-one

: 1432023-97-6
2-(4-chloro-3-methylphenyl)-2-oxoethyl (3-{[(benzyloxy)carbonyl]amino}oxetan-3-yl)acetate

Guidance literature:: With caesium carbonate; In acetonitrile; at 20 ℃; for 2h;

Reference yield:

: 1207175-54-9
3-amino-3-oxetaneacetic acid ethyl ester

: 1432023-97-6
2-(4-chloro-3-methylphenyl)-2-oxoethyl (3-{[(benzyloxy)carbonyl]amino}oxetan-3-yl)acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium carbonate / tert-butyl methyl ether / 5 - 20 °C / Large scale

1.2: 18 h / Large scale

2.1: caesium carbonate / acetonitrile / 2 h / 20 °C

With sodium carbonate; caesium carbonate; In tert-butyl methyl ether; acetonitrile;

Reference yield:

: 922500-91-2
ethyl 2-(oxetan-3-ylidene)acetate

: 1432023-97-6
2-(4-chloro-3-methylphenyl)-2-oxoethyl (3-{[(benzyloxy)carbonyl]amino}oxetan-3-yl)acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: ammonia / ethanol / 5 h / 100 °C / Sealed tube

2.1: sodium carbonate / tert-butyl methyl ether / 5 - 20 °C / Large scale

2.2: 18 h / Large scale

3.1: caesium carbonate / acetonitrile / 2 h / 20 °C

With ammonia; sodium carbonate; caesium carbonate; In ethanol; tert-butyl methyl ether; acetonitrile;