1,5-anhydro-3-benzamido-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-α-L-lyxo-hex-1-enitol

Base Information

• Chemical Name: 1,5-anhydro-3-benzamido-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-α-L-lyxo-hex-1-enitol
• CAS No.: 138925-09-4
• Molecular Formula: C₂₁H₂₁NO₄
• Molecular Weight: 351.402

Synonyms:1,5-anhydro-3-benzamido-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-α-L-lyxo-hex-1-enitol

Chemical Property of 1,5-anhydro-3-benzamido-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-α-L-lyxo-hex-1-enitol

Chemical Property:

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Technology Process of 1,5-anhydro-3-benzamido-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-α-L-lyxo-hex-1-enitol

There total 2 articles about 1,5-anhydro-3-benzamido-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-α-L-lyxo-hex-1-enitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

methyl 3-benzamido-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-α-L-lyxo-hexopyranoside (37091-14-8) → 1,5-anhydro-3-benzamido-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-α-L-lyxo-hex-1-enitol (138925-09-4)

Guidance literature:

With camphor-10-sulfonic acid; In benzene; for 12h; Heating;

Reference yield:

benzoyl chloride (98-88-4) → 1,5-anhydro-3-benzamido-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-α-L-lyxo-hex-1-enitol (138925-09-4)

Guidance literature:

Multi-step reaction with 2 steps

2: 100 percent / camphorsulfonic acid / benzene / 12 h / Heating

With camphor-10-sulfonic acid; In benzene;

Reference yield: 64.0%

phenyl 3,4,6-tri-O-benzyl-β-D-glucopyranoside (135192-39-1) + 1,5-anhydro-3-benzamido-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-α-L-lyxo-hex-1-enitol (138925-09-4) → phenyl O-(3-benzamido-4-O-benzoyl-2,3,6-tri-O-trideoxy-3-C-methyl-α-L-lyxo-hexopyranosyl)-(1-2)-3,4,6-tri-O-benzyl-β-D-glucopyranoside (138925-12-9)

Guidance literature:

With camphor-10-sulfonic acid; In benzene; for 16h; Ambient temperature;

upstream raw materials:

methyl 3-benzamido-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-α-L-lyxo-hexopyranoside

benzoyl chloride

Downstream raw materials:

Benzoic acid (1R,5R,7S,8S,9S)-9-iodo-1,7-dimethyl-3-phenyl-4,6-dioxa-2-aza-bicyclo[3.3.1]non-2-en-8-yl ester

phenyl O-(3-benzamido-4-O-benzoyl-2,3,6-tri-O-trideoxy-3-C-methyl-α-L-lyxo-hexopyranosyl)-(1-2)-3,4,6-tri-O-benzyl-β-D-glucopyranoside

2',6'-dimethoxyphenyl O-(3-benzamido-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-α-L-lyxo-hexopyranosyl)-(1-2)-3,4,6-tri-O-benzyl-β-D-glucopyranoside

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