α-<(3-(4-Chlorphenyl)-1,2,4-triazol-5-yl)-thio>acetessigsaeureethylester

Base Information

Chemical Name:α-<(3-(4-Chlorphenyl)-1,2,4-triazol-5-yl)-thio>acetessigsaeureethylester
CAS No.:132557-24-5
Molecular Formula:C₁₄H₁₄ClN₃O₃S
Molecular Weight:339.802
Hs Code.:

Synonyms:α-<(3-(4-Chlorphenyl)-1,2,4-triazol-5-yl)-thio>acetessigsaeureethylester

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Chemical Property of α-<(3-(4-Chlorphenyl)-1,2,4-triazol-5-yl)-thio>acetessigsaeureethylester

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Technology Process of α-<(3-(4-Chlorphenyl)-1,2,4-triazol-5-yl)-thio>acetessigsaeureethylester

There total 4 articles about α-<(3-(4-Chlorphenyl)-1,2,4-triazol-5-yl)-thio>acetessigsaeureethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 26028-65-9
5-(4-chlorophenyl)-3-mercapto-1,2,4-triazole

: 609-15-4
ethyl 2-chloro-3-oxo-butyrate

: 132557-24-5
α-<(3-(4-Chlorphenyl)-1,2,4-triazol-5-yl)-thio>acetessigsaeureethylester

Guidance literature:: With potassium hydroxide; for 1h; Heating;

Reference yield:

: 122-01-0
4-chloro-benzoyl chloride

: 132557-24-5
α-<(3-(4-Chlorphenyl)-1,2,4-triazol-5-yl)-thio>acetessigsaeureethylester

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / dichloromethane / 2 h / 0 - 15 °C

2: sodium hydroxide / 2 h / Reflux

3: potassium hydroxide / 1 h / Heating

With pyridine; potassium hydroxide; sodium hydroxide; In dichloromethane;