tert-butoxy-(2-methyl-4-p-tolyl-6,7,8,9-tetrahydro-benzo[g]quinolin-3-yl)-acetic acid ethyl ester

Base Information

Chemical Name:tert-butoxy-(2-methyl-4-p-tolyl-6,7,8,9-tetrahydro-benzo[g]quinolin-3-yl)-acetic acid ethyl ester
CAS No.:1377567-60-6
Molecular Formula:C₂₉H₃₅NO₃
Molecular Weight:445.602
Hs Code.:

Synonyms:tert-butoxy-(2-methyl-4-p-tolyl-6,7,8,9-tetrahydro-benzo[g]quinolin-3-yl)-acetic acid ethyl ester

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Chemical Property of tert-butoxy-(2-methyl-4-p-tolyl-6,7,8,9-tetrahydro-benzo[g]quinolin-3-yl)-acetic acid ethyl ester

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Technology Process of tert-butoxy-(2-methyl-4-p-tolyl-6,7,8,9-tetrahydro-benzo[g]quinolin-3-yl)-acetic acid ethyl ester

There total 6 articles about tert-butoxy-(2-methyl-4-p-tolyl-6,7,8,9-tetrahydro-benzo[g]quinolin-3-yl)-acetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.8%

: 540-88-5
acetic acid tert-butyl ester

: 1377567-59-3
hydroxy-(2-methyl-4-p-tolyl-6,7,8,9-tetrahydro-benzo[g]quinolin-3-yl)-acetic acid ethyl ester

: 1377567-60-6
tert-butoxy-(2-methyl-4-p-tolyl-6,7,8,9-tetrahydro-benzo[g]quinolin-3-yl)-acetic acid ethyl ester

Guidance literature:: acetic acid tert-butyl ester; hydroxy-(2-methyl-4-p-tolyl-6,7,8,9-tetrahydro-benzo[g]quinolin-3-yl)-acetic acid ethyl ester; With perchloric acid; at 20 ℃; for 3h; Inert atmosphere;

With sodium carbonate;

Reference yield:

: 615-79-2
ethyl 2,4-diketopentanoate

: 1377567-60-6
tert-butoxy-(2-methyl-4-p-tolyl-6,7,8,9-tetrahydro-benzo[g]quinolin-3-yl)-acetic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: chloro-trimethyl-silane / N,N-dimethyl-formamide / 2 h / 60 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: perchloric acid / 3 h / 20 °C / Inert atmosphere

With chloro-trimethyl-silane; perchloric acid; In N,N-dimethyl-formamide;

Reference yield:

: 104877-13-6
3-amino-5,6,7,8-tetrahydro-napthalene-2-carboxylic acid

: 1377567-60-6
tert-butoxy-(2-methyl-4-p-tolyl-6,7,8,9-tetrahydro-benzo[g]quinolin-3-yl)-acetic acid ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium carbonate / N,N-dimethyl-formamide / 20 °C / Inert atmosphere; Cooling with ice

2.1: dichloromethane; tetrahydrofuran / -78 - 20 °C / Inert atmosphere

2.2: -42 - 20 °C / Saturated solution

3.1: sodium hydroxide; water / ethanol; tetrahydrofuran / Inert atmosphere; Reflux

4.1: chloro-trimethyl-silane / N,N-dimethyl-formamide / 2 h / 60 °C / Inert atmosphere

4.2: 20 °C / Inert atmosphere

5.1: perchloric acid / 3 h / 20 °C / Inert atmosphere

With chloro-trimethyl-silane; perchloric acid; water; sodium carbonate; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;