C₉H₈F₂⁽¹⁸⁾FNO

Base Information

Chemical Name:C₉H₈F₂⁽¹⁸⁾FNO
CAS No.:1436389-39-7
Molecular Formula:C₉H₈F₃NO
Molecular Weight:202.165
Hs Code.:

C<sub>9</sub>H<sub>8</sub>F<sub>2</sub><sup>(18)</sup>FNO

Synonyms:C₉H₈F₂⁽¹⁸⁾FNO

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₉H₈F₂⁽¹⁸⁾FNO

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Technology Process of C₉H₈F₂⁽¹⁸⁾FNO

There total 6 articles about C₉H₈F₂⁽¹⁸⁾FNO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 1436389-33-1
[4-(acetylamino)phenyl](difluoro)acetic acid

: 1436389-39-7
C₉H₈F₂⁽¹⁸⁾FNO

Guidance literature:: With ⁽¹⁸⁾F-1-fluoro-4-chloromethyl-1,4-diazoniabicyclo[2.2.2]octane ditriflate; silver nitrate; In water; acetone; at 55 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ol4009377

Reference yield:

: 1514-87-0
metyhyl chlorodifluoroacetate

: 622-50-4
4-Acetamido-1-iodobenzene

: 1436389-39-7
C₉H₈F₂⁽¹⁸⁾FNO

Guidance literature:: With copper(l) iodide; 4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]hexacosan/[18F]fluoride; N,N,N,N,-tetramethylethylenediamine; In N,N-dimethyl-formamide; acetonitrile; at 100 - 150 ℃; for 0.333333h; regioselective reaction; Inert atmosphere; Sealed tube;
DOI:10.1038/nchem.1756

Reference yield:

: 622-50-4
4-Acetamido-1-iodobenzene

: 1436389-39-7
C₉H₈F₂⁽¹⁸⁾FNO

Guidance literature:: Multi-step reaction with 3 steps

1: copper / dimethyl sulfoxide / 12 h / 60 °C / Inert atmosphere

2: potassium carbonate / methanol; water / 2 h / 20 °C / Inert atmosphere

3: silver nitrate; ⁽¹⁸⁾F-1-fluoro-4-chloromethyl-1,4-diazoniabicyclo[2.2.2]octane ditriflate / water; acetone / 0.5 h / 55 °C / Inert atmosphere

With ⁽¹⁸⁾F-1-fluoro-4-chloromethyl-1,4-diazoniabicyclo[2.2.2]octane ditriflate; copper; potassium carbonate; silver nitrate; In methanol; water; dimethyl sulfoxide; acetone;
DOI:10.1021/ol4009377